N-<3-(ethoxycarbonyl)-2-benzylidene-1-oxopropyl>-L-alanine tert-butyl ester

Base Information

Chemical Name:N-<3-(ethoxycarbonyl)-2-benzylidene-1-oxopropyl>-L-alanine tert-butyl ester
CAS No.:96896-87-6
Molecular Formula:C₂₀H₂₇NO₅
Molecular Weight:361.438
Hs Code.:

Synonyms:N-<3-(ethoxycarbonyl)-2-benzylidene-1-oxopropyl>-L-alanine tert-butyl ester

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Chemical Property of N-<3-(ethoxycarbonyl)-2-benzylidene-1-oxopropyl>-L-alanine tert-butyl ester

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Technology Process of N-<3-(ethoxycarbonyl)-2-benzylidene-1-oxopropyl>-L-alanine tert-butyl ester

There total 1 articles about N-<3-(ethoxycarbonyl)-2-benzylidene-1-oxopropyl>-L-alanine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 21691-50-9
Ala-OtBu

: 87439-00-7
3-(ethoxycarbonyl)-2-benzylidenepropanoic acid

: 96896-87-6
N-<3-(ethoxycarbonyl)-2-benzylidene-1-oxopropyl>-L-alanine tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; chloroform; Ambient temperature;
DOI:10.1021/jm00147a007

Reference yield: 89.0%

: 96896-87-6
N-<3-(ethoxycarbonyl)-2-benzylidene-1-oxopropyl>-L-alanine tert-butyl ester

: 96896-88-7
N-(3-carboxy-2-benzylidene-1-oxopropyl)-L-alanine tert-butyl ester

Guidance literature:: With sodium hydroxide; In ethanol; for 4h; Ambient temperature;
DOI:10.1021/jm00147a007

Reference yield:

: 96896-87-6
N-<3-(ethoxycarbonyl)-2-benzylidene-1-oxopropyl>-L-alanine tert-butyl ester

: 92175-57-0,118867-26-8
Kelatorphan

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / 1 N aq. NaOH / ethanol / 4 h / Ambient temperature

2: 96 percent / Et₃N,1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

3: 50 percent / TFA / 1 h / Ambient temperature

4: H₂ / 10percent Pd on charcoal / methanol / 3 h / Ambient temperature

With sodium hydroxide; hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; chloroform;
DOI:10.1021/jm00147a007