C₄₇H₃₃N₃

Base Information

Chemical Name:C₄₇H₃₃N₃
CAS No.:1373227-19-0
Molecular Formula:C₄₇H₃₃N₃
Molecular Weight:639.799
Hs Code.:

C<sub>47</sub>H<sub>33</sub>N<sub>3</sub>

Synonyms:C₄₇H₃₃N₃

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Chemical Property of C₄₇H₃₃N₃

Chemical Property:

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Technology Process of C₄₇H₃₃N₃

There total 7 articles about C₄₇H₃₃N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.4%

: 1262866-93-2
4-([1,1‘-biphenyl]-4-yl)-2-chloroquinazoline

: 1373227-16-7
C₂₇H₂₂BNO₂

: 1373227-19-0
C₄₇H₃₃N₃

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; at 120 ℃; for 24h;

Reference yield: 60.0%

: 1373227-19-0
C₄₇H₃₃N₃

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 120 ℃; for 12h;

Reference yield:

: 333432-28-3
9,9-dimethyl-9H-fluoren-2-yl-2-boronic acid

: 1373227-19-0
C₄₇H₃₃N₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 6 h / 120 °C

2.1: triethyl phosphite / 1,2-dichloro-benzene / 24 h / 160 °C

3.1: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / toluene / 72 h / 90 °C

4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.2: 5 h / Inert atmosphere

4.3: Inert atmosphere

5.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / 120 °C

With n-butyllithium; sodium carbonate; sodium t-butanolate; triethyl phosphite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium diacetate; In tetrahydrofuran; ethanol; hexane; water; 1,2-dichloro-benzene; toluene; 1.1: Suzuki Coupling / 3.1: Buchwald reaction;