2-(10-[1,3]Dithiol-2-ylidene-10H-anthracen-9-ylidene)-4-octadecylsulfanyl-5-p-tolyl-[1,3]dithiole

Base Information

Chemical Name:2-(10-[1,3]Dithiol-2-ylidene-10H-anthracen-9-ylidene)-4-octadecylsulfanyl-5-p-tolyl-[1,3]dithiole
CAS No.:128315-75-3
Molecular Formula:C₄₅H₅₄S₅
Molecular Weight:755.254
Hs Code.:

Synonyms:2-(10-[1,3]Dithiol-2-ylidene-10H-anthracen-9-ylidene)-4-octadecylsulfanyl-5-p-tolyl-[1,3]dithiole

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Chemical Property of 2-(10-[1,3]Dithiol-2-ylidene-10H-anthracen-9-ylidene)-4-octadecylsulfanyl-5-p-tolyl-[1,3]dithiole

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Technology Process of 2-(10-[1,3]Dithiol-2-ylidene-10H-anthracen-9-ylidene)-4-octadecylsulfanyl-5-p-tolyl-[1,3]dithiole

There total 3 articles about 2-(10-[1,3]Dithiol-2-ylidene-10H-anthracen-9-ylidene)-4-octadecylsulfanyl-5-p-tolyl-[1,3]dithiole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 109857-93-4
10-(1,3-dithiol-2-ylidene)anthracene-9⁽¹⁰⁾H-one

: 128315-82-2
(4-Octadecylsulfanyl-5-p-tolyl-[1,3]dithiol-2-yl)-phosphonic acid dimethyl ester

: 128315-75-3
2-(10-[1,3]Dithiol-2-ylidene-10H-anthracen-9-ylidene)-4-octadecylsulfanyl-5-p-tolyl-[1,3]dithiole

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 ℃;
DOI:10.1039/c39900000470

Reference yield:

: 90-44-8
anthracen-9(10H)-one

: 128315-75-3
2-(10-[1,3]Dithiol-2-ylidene-10H-anthracen-9-ylidene)-4-octadecylsulfanyl-5-p-tolyl-[1,3]dithiole

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridine, acetic acid / Heating

2: 55 percent / n-butyl lithium / tetrahydrofuran / -78 °C

With pyridine; n-butyllithium; acetic acid; In tetrahydrofuran;
DOI:10.1039/c39900000470

Reference yield:

: 128315-79-7
2-Ethoxy-4-octadecylsulfanyl-5-p-tolyl-[1,3]dithiole

: 128315-75-3
2-(10-[1,3]Dithiol-2-ylidene-10H-anthracen-9-ylidene)-4-octadecylsulfanyl-5-p-tolyl-[1,3]dithiole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) tetrafluoroboric acid, 2.) sodium iodide / 1.) ether, 0 deg C, 2.) acetonitrile, 20 deg C

2: 55 percent / n-butyl lithium / tetrahydrofuran / -78 °C

With tetrafluoroboric acid; n-butyllithium; sodium iodide; In tetrahydrofuran;
DOI:10.1039/c39900000470