N-(1,1-dimethylethyl)-1,1-dimethyl-1-(1,5,6,7-tetrahydro-2-methyl-4-phenyl-s-2-indacen-1-yl)silanamine

Base Information

Chemical Name:N-(1,1-dimethylethyl)-1,1-dimethyl-1-(1,5,6,7-tetrahydro-2-methyl-4-phenyl-s-2-indacen-1-yl)silanamine
CAS No.:656800-70-3
Molecular Formula:C₂₅H₃₃NSi
Molecular Weight:375.629
Hs Code.:

Synonyms:N-(1,1-dimethylethyl)-1,1-dimethyl-1-(1,5,6,7-tetrahydro-2-methyl-4-phenyl-s-2-indacen-1-yl)silanamine

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Chemical Property of N-(1,1-dimethylethyl)-1,1-dimethyl-1-(1,5,6,7-tetrahydro-2-methyl-4-phenyl-s-2-indacen-1-yl)silanamine

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Technology Process of N-(1,1-dimethylethyl)-1,1-dimethyl-1-(1,5,6,7-tetrahydro-2-methyl-4-phenyl-s-2-indacen-1-yl)silanamine

There total 1 articles about N-(1,1-dimethylethyl)-1,1-dimethyl-1-(1,5,6,7-tetrahydro-2-methyl-4-phenyl-s-2-indacen-1-yl)silanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: dimethyl(t-butylamino)silylchloride

: 852160-02-2
6-methyl-4-phenyl-1,2,3,5-tetrahydro-s-indacene

: 656800-70-3
N-(1,1-dimethylethyl)-1,1-dimethyl-1-(1,5,6,7-tetrahydro-2-methyl-4-phenyl-s-2-indacen-1-yl)silanamine

Guidance literature:: 6-methyl-4-phenyl-1,2,3,5-tetrahydro-s-indacene; With n-butyllithium; In hexanes; for 1h;

dimethyl(t-butylamino)silylchloride; In tetrahydrofuran; for 16 - 18h;

Reference yield: 59.0%

: 31168-87-3,18039-90-2
titanium trichloride tris(tetrahydrofuran)

: 656800-70-3
N-(1,1-dimethylethyl)-1,1-dimethyl-1-(1,5,6,7-tetrahydro-2-methyl-4-phenyl-s-2-indacen-1-yl)silanamine

: dichloro[N-(1,1-dimethylethyl)-1,1-dimethyl-[(1,2,3,3a,8a-η)-1,5,6,7-tetrahydro-2-methyl-4-phenyl-s-indacen-1-yl]silanaminato(2-)-N]titanium

Guidance literature:: N-(1,1-dimethylethyl)-1,1-dimethyl-1-(1,5,6,7-tetrahydro-2-methyl-4-phenyl-s-2-indacen-1-yl)silanamine; With n-butyllithium; In hexanes; hexane; for 1.5h;

titanium trichloride tris(tetrahydrofuran); In tetrahydrofuran; hexanes; hexane; at -30 - 25 ℃; for 0.416667h;

With lead(II) chloride; In tetrahydrofuran; hexanes; hexane; for 2h;