2-Benzylamino-1--aethanol

Base Information

• Chemical Name: 2-Benzylamino-1--aethanol
• CAS No.: 93026-74-5
• Molecular Formula: C₁₆H₁₉NO
• Molecular Weight: 241.333

Synonyms:2-Benzylamino-1--aethanol

Chemical Property of 2-Benzylamino-1--aethanol

Chemical Property:

Purity/Quality:

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Technology Process of 2-Benzylamino-1--aethanol

There total 3 articles about 2-Benzylamino-1--aethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-methylphenyl)oxirane (13107-39-6) + benzylamine (100-46-9) → 2-Benzylamino-1--aethanol (93026-74-5) + 2-Benzylamino-2--aethanol (94708-10-8)

Guidance literature:

With activated silica; for 24h; regioselective reaction; Inert atmosphere;

DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

2-(4-methylphenyl)oxirane (13107-39-6) + benzylamine (100-46-9) → 2-Benzylamino-1--aethanol (93026-74-5)

Guidance literature:

In ethanol; at 140 ℃; for 0.166667h; Inert atmosphere; Sealed tube; Microwave irradiation;

DOI:10.1021/acs.orglett.1c01821

Reference yield:

→ 2-Benzylamino-1--aethanol (93026-74-5)

Guidance literature:

1.) 4-Methyl-phenacylbromid, Benzylamin, Molverh. 1:2, Dioxan, 5 min., 60gradC -> Aminoketon, 2.) NaBH4, W.;

upstream raw materials:

2-(4-methylphenyl)oxirane

benzylamine

Downstream raw materials:

C₂₁H₂₇NO₃

2-(benzyl(tert-butoxycarbonyl)amino)-1-p-tolylethyl 2,6-dichlorobenzenesulfonate

2-(benzyl(tert-butoxycarbonyl)amino)-1-p-tolylethyl 2,3-dichlorobenzenesulfonate

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