Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl)-β-D-ribofuranosid

Base Information

Chemical Name:Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl)-β-D-ribofuranosid
CAS No.:78416-63-4
Molecular Formula:C₃₅H₄₂O₁₅
Molecular Weight:702.709
Hs Code.:

Synonyms:Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl)-β-D-ribofuranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl)-β-D-ribofuranosid

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Technology Process of Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl)-β-D-ribofuranosid

There total 6 articles about Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl)-β-D-ribofuranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 29741-69-3
3,4,6-tetra-O-acetyl-2-O-benzyl-α-D-glucopyranosyl bromide

: 78416-51-0
Benzyl-2,3-di-O-acetyl-β-D-ribofuranosid

: 78416-63-4
Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl)-β-D-ribofuranosid

: 78416-63-4
Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-β-D-ribofuranosid

Guidance literature:: With mercury(II) cyanide; mercury dibromide; In benzene; at 50 ℃; for 18h; Yields of byproduct given;

Reference yield: 80.0%

: 29741-69-3
3,4,6-tetra-O-acetyl-2-O-benzyl-α-D-glucopyranosyl bromide

: 78416-51-0
Benzyl-2,3-di-O-acetyl-β-D-ribofuranosid

: 78416-63-4
Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl)-β-D-ribofuranosid

: 78416-63-4
Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-β-D-ribofuranosid

Guidance literature:: With mercury(II) cyanide; mercury dibromide; In benzene; at 50 ℃; for 18h; Yields of byproduct given;

Reference yield:

: 54946-48-4
benzyl-β-D-ribofuranoside

: 78416-63-4
Benzyl-2,3-di-O-acetyl-5-O-(3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl)-β-D-ribofuranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 2) NaOAc / 1) pyridine, 30-36 deg C, 24 h, 2) pyridine, 20-22 deg C, 18 h

2: 77 percent / 1 M HCl / dioxane / 20 °C

3: Hg(CN)2, HgBr₂ / benzene / 18 h / 50 °C

With hydrogenchloride; sodium acetate; mercury(II) cyanide; mercury dibromide; In 1,4-dioxane; benzene;