4-(3-(N,N-di(4-methylbenzyl)amino)phenyl)-1-(4-methylbenzyl)-1H-1,2,3-triazole

Base Information

• Chemical Name: 4-(3-(N,N-di(4-methylbenzyl)amino)phenyl)-1-(4-methylbenzyl)-1H-1,2,3-triazole
• CAS No.: 1595281-87-0
• Molecular Formula: C₃₂H₃₂N₄
• Molecular Weight: 472.633
• Mol file: 1595281-87-0.mol

Synonyms:4-(3-(N,N-di(4-methylbenzyl)amino)phenyl)-1-(4-methylbenzyl)-1H-1,2,3-triazole

Chemical Property of 4-(3-(N,N-di(4-methylbenzyl)amino)phenyl)-1-(4-methylbenzyl)-1H-1,2,3-triazole

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-(3-(N,N-di(4-methylbenzyl)amino)phenyl)-1-(4-methylbenzyl)-1H-1,2,3-triazole

There total 4 articles about 4-(3-(N,N-di(4-methylbenzyl)amino)phenyl)-1-(4-methylbenzyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-(3-aminophenyl)-1-(4-methylbenzyl)-1H-1,2,3-triazole + 4-Methylbenzyl bromide (104-81-4) → 4-(3-(N,N-di(4-methylbenzyl)amino)phenyl)-1-(4-methylbenzyl)-1H-1,2,3-triazole (1595281-87-0)

Guidance literature:

With copper; In methanol; at 20 ℃;

DOI:10.3987/COM-15-13277

Reference yield: 87.0%

3-acetylenephenylamine (54060-30-9) + 4-Methylbenzyl bromide (104-81-4) → 4-(3-(N,N-di(4-methylbenzyl)amino)phenyl)-1-(4-methylbenzyl)-1H-1,2,3-triazole (1595281-87-0)

Guidance literature:

With sodium azide; copper; In methanol; at 20 ℃; for 6h; Reagent/catalyst; regioselective reaction;

DOI:10.3987/COM-15-13277

Reference yield: 82.0%

3-acetylenephenylamine (54060-30-9) + 4-Methylbenzyl chloride (104-82-5) → 4-(3-(N,N-di(4-methylbenzyl)amino)phenyl)-1-(4-methylbenzyl)-1H-1,2,3-triazole (1595281-87-0)

Guidance literature:

With sodium azide; copper; In methanol; at 20 ℃; for 14h; regioselective reaction;

DOI:10.1016/j.tetlet.2014.02.114

upstream raw materials:

3-acetylenephenylamine

4-Methylbenzyl chloride

4-Methylbenzyl bromide