[1-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-meth-(E)-ylidene]-(6-bromomethyl-2,4-dimethyl-5,6-dihydro-pyrrolo[2,3-d]pyrimidin-7-yl)-amine; hydrobromide

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Chemical Name:[1-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-meth-(E)-ylidene]-(6-bromomethyl-2,4-dimethyl-5,6-dihydro-pyrrolo[2,3-d]pyrimidin-7-yl)-amine; hydrobromide
CAS No.:98189-80-1
Molecular Formula:BrH*C₂₀H₂₄BrCl₂N₅
Molecular Weight:566.166
Hs Code.:

Synonyms:[1-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-meth-(E)-ylidene]-(6-bromomethyl-2,4-dimethyl-5,6-dihydro-pyrrolo[2,3-d]pyrimidin-7-yl)-amine; hydrobromide

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Chemical Property of [1-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-meth-(E)-ylidene]-(6-bromomethyl-2,4-dimethyl-5,6-dihydro-pyrrolo[2,3-d]pyrimidin-7-yl)-amine; hydrobromide

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Technology Process of [1-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-meth-(E)-ylidene]-(6-bromomethyl-2,4-dimethyl-5,6-dihydro-pyrrolo[2,3-d]pyrimidin-7-yl)-amine; hydrobromide

There total 3 articles about [1-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-meth-(E)-ylidene]-(6-bromomethyl-2,4-dimethyl-5,6-dihydro-pyrrolo[2,3-d]pyrimidin-7-yl)-amine; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 98189-71-0
{4-[(5-Allyl-2,6-dimethyl-pyrimidin-4-yl)-hydrazonomethyl]-phenyl}-bis-(2-chloro-ethyl)-amine

: 98189-80-1
[1-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-meth-(E)-ylidene]-(6-bromomethyl-2,4-dimethyl-5,6-dihydro-pyrrolo[2,3-d]pyrimidin-7-yl)-amine; hydrobromide

Guidance literature:: With bromine; In chloroform; for 0.75h; Ambient temperature;
DOI:10.1007/BF00506076

Reference yield:

: 98189-66-3
5-allyl-4-hydrazino-3,6-dimethylpyrimidine

: 98189-80-1
[1-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-meth-(E)-ylidene]-(6-bromomethyl-2,4-dimethyl-5,6-dihydro-pyrrolo[2,3-d]pyrimidin-7-yl)-amine; hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / methanol / 0.67 h / Heating

2: 70 percent / Br₂ / CHCl₃ / 0.75 h / Ambient temperature

With bromine; In methanol; chloroform;
DOI:10.1007/BF00506076

Reference yield:

: 81401-28-7
2,4-dimethyl-5-allyl-6-chloropyrimidine

: 98189-80-1
[1-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-meth-(E)-ylidene]-(6-bromomethyl-2,4-dimethyl-5,6-dihydro-pyrrolo[2,3-d]pyrimidin-7-yl)-amine; hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / hydrazine hydrate / methanol / 8 h / Heating

2: 96 percent / methanol / 0.67 h / Heating

3: 70 percent / Br₂ / CHCl₃ / 0.75 h / Ambient temperature

With bromine; hydrazine hydrate; In methanol; chloroform;
DOI:10.1007/BF00506076