C₂₅H₂₁NO₄S₂

Base Information

Chemical Name:C₂₅H₂₁NO₄S₂
CAS No.:1374831-50-1
Molecular Formula:C₂₅H₂₁NO₄S₂
Molecular Weight:463.578
Hs Code.:

C<sub>25</sub>H<sub>21</sub>NO<sub>4</sub>S<sub>2</sub>

Synonyms:C₂₅H₂₁NO₄S₂

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Chemical Property of C₂₅H₂₁NO₄S₂

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Technology Process of C₂₅H₂₁NO₄S₂

There total 3 articles about C₂₅H₂₁NO₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₂₁NO₆S₂

: 1374831-50-1
C₂₅H₂₁NO₄S₂

Guidance literature:: With caesium carbonate; palladium dichloride; tri tert-butylphosphoniumtetrafluoroborate; In N,N-dimethyl-formamide; at 170 ℃; for 0.133333h; regioselective reaction; Microwave irradiation; Inert atmosphere;
DOI:10.1021/ol3009655

Reference yield:

: 1374831-33-0
C₂₇H₂₃NO₆S₂

: 1374831-50-1
C₂₅H₂₁NO₄S₂

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / tetrahydrofuran; methanol; water / 1 h / 80 °C

2: caesium carbonate; palladium dichloride; tri tert-butylphosphoniumtetrafluoroborate / N,N-dimethyl-formamide / 0.13 h / 170 °C / Microwave irradiation; Inert atmosphere

With caesium carbonate; sodium hydroxide; palladium dichloride; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol3009655

Reference yield:

: 1374831-20-5
methyl 3-((N-(2-bromobenzyl)-4-methoxyphenyl)sulfonamido)thiophene-2-carboxylate

: 1374831-50-1
C₂₅H₂₁NO₄S₂

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; potassium carbonate; trimethylpyruvic acid; tricyclohexylphosphine tetrafluoroborate / 2,4-dichlorophenoxyacetic acid dimethylamine / 16 h / 100 °C

2: sodium hydroxide / tetrahydrofuran; methanol; water / 1 h / 80 °C

3: caesium carbonate; palladium dichloride; tri tert-butylphosphoniumtetrafluoroborate / N,N-dimethyl-formamide / 0.13 h / 170 °C / Microwave irradiation; Inert atmosphere

With palladium diacetate; potassium carbonate; caesium carbonate; trimethylpyruvic acid; tricyclohexylphosphine tetrafluoroborate; sodium hydroxide; palladium dichloride; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; methanol; water; 2,4-dichlorophenoxyacetic acid dimethylamine; N,N-dimethyl-formamide;
DOI:10.1021/ol3009655