C₄₁H₄₁Br₂N₇O₇

Base Information

Chemical Name:C₄₁H₄₁Br₂N₇O₇
CAS No.:1262657-46-4
Molecular Formula:C₄₁H₄₁Br₂N₇O₇
Molecular Weight:903.627
Hs Code.:

C<sub>41</sub>H<sub>41</sub>Br<sub>2</sub>N<sub>7</sub>O<sub>7</sub>

Synonyms:C₄₁H₄₁Br₂N₇O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₄₁Br₂N₇O₇

Chemical Property:

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Technology Process of C₄₁H₄₁Br₂N₇O₇

There total 18 articles about C₄₁H₄₁Br₂N₇O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50371-52-3
4,5-dibromopyrrol-2-yl trichloromethyl ketone

: 1262657-49-7
C₂HF₃O₂*C₃₆H₄₀N₆O₆

: 1262657-46-4
C₄₁H₄₁Br₂N₇O₇

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 70 ℃; for 5h;
DOI:10.1039/c0cc02214d

Reference yield:

: 1262657-45-3
C₃₆H₃₈N₈O₆

: 1262657-46-4
C₄₁H₄₁Br₂N₇O₇

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / tetrahydrofuran; water / 1 h / 80 °C

1.2: 23 °C

2.1: triethylamine / N,N-dimethyl-formamide / 5 h / 70 °C

With triethylamine; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide; 1.1: Staudinger reaction;
DOI:10.1039/c0cc02214d

Reference yield:

: C₁₉H₂₀N₂O₃

: 1262657-46-4
C₄₁H₄₁Br₂N₇O₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: trichlorophosphate / mineral oil / 2 h / 0 - 23 °C / Inert atmosphere

1.2: 1 h / 23 °C / Cooling with ice

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

2.2: 2 h / -78 °C

3.1: Dess-Martin periodane / dichloromethane; water / 2 h / 23 °C

4.1: manganese(III) triacetate dihydrate; acetic acid / 0 - 60 °C / Inert atmosphere

5.1: lithium hydroxide / tetrahydrofuran; water / 0.5 h / 23 °C

5.2: 0 - 23 °C / Inert atmosphere

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 - 0 °C

7.1: calcium borohydride bis(tetrahydrofuran) / tetrahydrofuran / 0.5 h / 0 - 23 °C

7.2: 0.5 h / 0 - 50 °C

8.1: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

9.1: water; Dess-Martin periodane / dichloromethane / 0.25 h / 40 °C

10.1: hydrogenchloride / methanol; water / 2 h / 0 - 40 °C

11.1: potassium hydrogen phthalate / methanol; water / 10 - 15 °C / pH 3.7

11.2: 110 °C

12.1: triphenylphosphine / tetrahydrofuran; water / 1 h / 80 °C

12.2: 23 °C

13.1: triethylamine / N,N-dimethyl-formamide / 5 h / 70 °C

With hydrogenchloride; calcium borohydride bis(tetrahydrofuran); water; potassium hydrogen phthalate; manganese(III) triacetate dihydrate; Dess-Martin periodane; acetic acid; triethylamine; triphenylphosphine; trifluoroacetic acid; lithium hydroxide; lithium hexamethyldisilazane; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; 5.2: Mitsunobu reaction / 12.1: Staudinger reaction;
DOI:10.1039/c0cc02214d