5-(phenylthio)-1-iodopentane

Base Information

• Chemical Name: 5-(phenylthio)-1-iodopentane
• CAS No.: 83705-76-4
• Molecular Formula: C₁₁H₁₅IS
• Molecular Weight: 306.211
• Mol file: 83705-76-4.mol

Synonyms:5-(phenylthio)-1-iodopentane

Chemical Property of 5-(phenylthio)-1-iodopentane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 5-(phenylthio)-1-iodopentane

There total 2 articles about 5-(phenylthio)-1-iodopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pent-4-en-1-yl phenyl sulfide (4285-51-2) → 5-(phenylthio)-1-iodopentane (83705-76-4)

Guidance literature:

pent-4-en-1-yl phenyl sulfide; With triisobutylaluminum; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; at 25 ℃; for 12h;

With iodine; In dichloromethane;

DOI:10.1016/S0040-4039(00)02142-0

Reference yield:

5-chloropentan-1-ol (5259-98-3) + thiophenol (108-98-5) → 5-(phenylthio)-1-iodopentane (83705-76-4)

Guidance literature:

With methanesulfonic acid; sodium iodide; Multistep reaction;

DOI:10.1021/jo00149a003

Reference yield:

5-(phenylthio)-1-iodopentane (83705-76-4) → S-phenylthianium iodide

Guidance literature:

for 336h; Ambient temperature;

DOI:10.1021/jo00149a003

upstream raw materials:

5-chloropentan-1-ol

thiophenol

pent-4-en-1-yl phenyl sulfide