benzyl 4-(3-oxo-3,5-dihydro-4H-1,4,8b-triazaacenaphthylen-4-yl)butylcarbamate

Base Information

Chemical Name:benzyl 4-(3-oxo-3,5-dihydro-4H-1,4,8b-triazaacenaphthylen-4-yl)butylcarbamate
CAS No.:312307-99-6
Molecular Formula:C₂₁H₂₂N₄O₃
Molecular Weight:378.431
Hs Code.:

Synonyms:benzyl 4-(3-oxo-3,5-dihydro-4H-1,4,8b-triazaacenaphthylen-4-yl)butylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 4-(3-oxo-3,5-dihydro-4H-1,4,8b-triazaacenaphthylen-4-yl)butylcarbamate

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Technology Process of benzyl 4-(3-oxo-3,5-dihydro-4H-1,4,8b-triazaacenaphthylen-4-yl)butylcarbamate

There total 2 articles about benzyl 4-(3-oxo-3,5-dihydro-4H-1,4,8b-triazaacenaphthylen-4-yl)butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 18807-73-3
N-benzyloxycarbonyl-1,4-butanediamine hydrochloride

: ethyl 5-(chloromethyl)imidazo[1,2-a]pyridine-3-carboxylate sulfuric acid salt

: 312307-99-6
benzyl 4-(3-oxo-3,5-dihydro-4H-1,4,8b-triazaacenaphthylen-4-yl)butylcarbamate

Guidance literature:: With sodium methylate; triethylamine; sodium iodide; In methanol; N,N-dimethyl-formamide; at 40 ℃; for 1h;
DOI:10.1016/S0040-4020(00)00709-2

Reference yield:

: 18807-73-3
N-benzyloxycarbonyl-1,4-butanediamine hydrochloride

: ethyl 5-(chloromethyl)imidazo[1,2-a]pyridine-3-carboxylate sulfuric acid salt

: 312307-99-6
benzyl 4-(3-oxo-3,5-dihydro-4H-1,4,8b-triazaacenaphthylen-4-yl)butylcarbamate

: [4-(3,5-dioxo-3,5-dihydro-1,4,8b-triaza-acenaphthylen-4-yl)-butyl]-carbamic acid benzyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 70 ℃; for 3h; Further Variations:; Reagents; Solvents; Temperatures; Product distribution;
DOI:10.1016/S0040-4020(00)00709-2