2,5-Bis-(iodomethyl-dimethyl-silanyl)-3,4-diphenyl-1,1-divinyl-1H-silole

Base Information

Chemical Name:2,5-Bis-(iodomethyl-dimethyl-silanyl)-3,4-diphenyl-1,1-divinyl-1H-silole
CAS No.:213009-81-5
Molecular Formula:C₂₆H₃₂I₂Si₃
Molecular Weight:682.606
Hs Code.:

Synonyms:2,5-Bis-(iodomethyl-dimethyl-silanyl)-3,4-diphenyl-1,1-divinyl-1H-silole

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Chemical Property of 2,5-Bis-(iodomethyl-dimethyl-silanyl)-3,4-diphenyl-1,1-divinyl-1H-silole

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Technology Process of 2,5-Bis-(iodomethyl-dimethyl-silanyl)-3,4-diphenyl-1,1-divinyl-1H-silole

There total 2 articles about 2,5-Bis-(iodomethyl-dimethyl-silanyl)-3,4-diphenyl-1,1-divinyl-1H-silole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 213009-79-1
2,5-Bis-(chloromethyl-dimethyl-silanyl)-3,4-diphenyl-1,1-divinyl-1H-silole

: 213009-81-5
2,5-Bis-(iodomethyl-dimethyl-silanyl)-3,4-diphenyl-1,1-divinyl-1H-silole

Guidance literature:: With sodium iodide; In butanone; for 24h; Heating;
DOI:10.1016/S0040-4020(98)00620-6

Reference yield:

: 197172-17-1
di-phenylethynyl-divinylsilane

: 213009-81-5
2,5-Bis-(iodomethyl-dimethyl-silanyl)-3,4-diphenyl-1,1-divinyl-1H-silole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LiC₁₀H₈ / 1.) THF, room temperature, 3 h, 2.) -70 deg C, 15 min, 3.) room temperature

2: 65 percent / NaI / butan-2-one / 24 h / Heating

With LiC₁₀H₈; sodium iodide; In butanone;
DOI:10.1016/S0040-4020(98)00620-6

Reference yield: 80.0%

: 213009-81-5
2,5-Bis-(iodomethyl-dimethyl-silanyl)-3,4-diphenyl-1,1-divinyl-1H-silole

: 3,4-Diphenyl-2,5-bis-trimethylsilanyl-1,1-divinyl-1H-silole

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 14h; Heating;
DOI:10.1016/S0040-4020(98)00620-6