methyl (E)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate

Base Information

Chemical Name:methyl (E)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate
CAS No.:125318-32-3
Molecular Formula:C₁₇H₂₄O₆
Molecular Weight:324.374
Hs Code.:

Synonyms:methyl (E)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate

Suppliers and Price of methyl (E)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl (E)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl (E)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate

There total 7 articles about methyl (E)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 26530-60-9
trimethyl 2-phosphonopropionate

: 125318-30-1
<2,5-bis(methoxymethoxy)-3-methylphenyl>acetaldehyde

: 125318-31-2
methyl (Z)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate

: 125318-32-3
methyl (E)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at -70 ℃; for 0.5h;
DOI:10.1016/S0040-4020(01)80058-2

Reference yield:

: 6293-55-6
2-bromo-6-methyl-[1,4]benzoquinone

: 125318-32-3
methyl (E)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate

Guidance literature:: Multi-step reaction with 5 steps

1: 38 percent / Na₂S₂O₄ / ethanol; H₂O / 1 h / 60 °C

2: 57 percent / Na / 2-methoxy-ethanol / Ambient temperature

3: 88 percent / n-BuLi, CuI / hexane; diethyl ether / Ambient temperature

4: 20 g / OsO₄, NaIO₄ / diethyl ether / 6 h / Ambient temperature

5: 25 percent / NaH / tetrahydrofuran / 0.5 h / -70 °C

With sodium periodate; copper(l) iodide; osmium(VIII) oxide; n-butyllithium; sodium dithionite; sodium; sodium hydride; In tetrahydrofuran; diethyl ether; ethanol; hexane; 2-methoxy-ethanol; water;
DOI:10.1016/S0040-4020(01)80058-2

Reference yield:

: 609-22-3
2,4-dibromo-6-methylphenol

: 125318-32-3
methyl (E)-4-<2,5-bis(methoxymethoxy)-3-methylphenyl>-2-methyl-2-butenoate

Guidance literature:: Multi-step reaction with 6 steps

1: 245 g / CrO₃ / acetic acid; H₂O / 5 h / 0 °C

2: 38 percent / Na₂S₂O₄ / ethanol; H₂O / 1 h / 60 °C

3: 57 percent / Na / 2-methoxy-ethanol / Ambient temperature

4: 88 percent / n-BuLi, CuI / hexane; diethyl ether / Ambient temperature

5: 20 g / OsO₄, NaIO₄ / diethyl ether / 6 h / Ambient temperature

6: 25 percent / NaH / tetrahydrofuran / 0.5 h / -70 °C

With chromium(VI) oxide; sodium periodate; copper(l) iodide; osmium(VIII) oxide; n-butyllithium; sodium dithionite; sodium; sodium hydride; In tetrahydrofuran; diethyl ether; ethanol; hexane; 2-methoxy-ethanol; water; acetic acid;
DOI:10.1016/S0040-4020(01)80058-2