biphenyl-4-yl 4-O-(dibenzyloxyphosphoryl)-2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside

Base Information

Chemical Name:biphenyl-4-yl 4-O-(dibenzyloxyphosphoryl)-2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside
CAS No.:1415481-58-1
Molecular Formula:C₅₃H₄₇O₁₁P
Molecular Weight:890.923
Hs Code.:

Synonyms:biphenyl-4-yl 4-O-(dibenzyloxyphosphoryl)-2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside

Suppliers and Price of biphenyl-4-yl 4-O-(dibenzyloxyphosphoryl)-2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of biphenyl-4-yl 4-O-(dibenzyloxyphosphoryl)-2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of biphenyl-4-yl 4-O-(dibenzyloxyphosphoryl)-2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside

There total 10 articles about biphenyl-4-yl 4-O-(dibenzyloxyphosphoryl)-2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1415481-57-0
biphenyl-4-yl 2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 1415481-58-1
biphenyl-4-yl 4-O-(dibenzyloxyphosphoryl)-2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside

Guidance literature:: biphenyl-4-yl 2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside; Dibenzyl N,N-diisopropylphosphoramidite; With 1,2,4-Triazole; In acetonitrile; at 0 - 20 ℃; for 16.3333h; Inert atmosphere;

With tert.-butylhydroperoxide; In acetonitrile; at 0 - 20 ℃; for 1h;

Reference yield:

: 31909-79-2,31909-80-5,120489-26-1,145875-00-9,134699-00-6
(2R,3S,4S,5S,6R)-2-(hydroxymethyl)-6-(4-phenylphenoxy)-tetrahydropyran-3,4,5-triol

: 1415481-58-1
biphenyl-4-yl 4-O-(dibenzyloxyphosphoryl)-2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide; acetonitrile / 80 °C

2.1: dmap / pyridine / 20 °C

3.1: ethane; aluminum (III) chloride / water; tetrahydrofuran / 1 h / 20 °C

4.1: 1,2,4-Triazole / acetonitrile / 16.33 h / 0 - 20 °C / Inert atmosphere

4.2: 1 h / 0 - 20 °C

With 1,2,4-Triazole; dmap; aluminum (III) chloride; ethane; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1415481-47-8
biphenyl-4-yl 4,6-O-benzylidene-α-D-mannopyranoside

: 1415481-58-1
biphenyl-4-yl 4-O-(dibenzyloxyphosphoryl)-2,3-di-O-benzoyl-6-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap / pyridine / 20 °C

2.1: ethane; aluminum (III) chloride / water; tetrahydrofuran / 1 h / 20 °C

3.1: 1,2,4-Triazole / acetonitrile / 16.33 h / 0 - 20 °C / Inert atmosphere

3.2: 1 h / 0 - 20 °C

With 1,2,4-Triazole; dmap; aluminum (III) chloride; ethane; In tetrahydrofuran; pyridine; water; acetonitrile;