Technology Process of C39H60N6O9
There total 6 articles about C39H60N6O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chloroformic acid ethyl ester; triethylamine;
In
tetrahydrofuran;
at -5 ℃;
DOI:10.1016/j.bmcl.2005.12.013
- Guidance literature:
-
Multi-step reaction with 5 steps
1: CH2Cl2
2: 77 percent / aq. LiOH / tetrahydrofuran
3: 90 percent / HATU; DIPEA / dimethylformamide / -20 °C
4: 100 percent / HCl / dioxane
5: 50 percent / EtOCOCl; Et3N / tetrahydrofuran / -5 °C
With
hydrogenchloride; lithium hydroxide; chloroformic acid ethyl ester; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
1: Passerini reaction;
DOI:10.1016/j.bmcl.2005.12.013
- Guidance literature:
-
Multi-step reaction with 6 steps
1: LAH / tetrahydrofuran / -30 °C
2: CH2Cl2
3: 77 percent / aq. LiOH / tetrahydrofuran
4: 90 percent / HATU; DIPEA / dimethylformamide / -20 °C
5: 100 percent / HCl / dioxane
6: 50 percent / EtOCOCl; Et3N / tetrahydrofuran / -5 °C
With
hydrogenchloride; lithium hydroxide; lithium aluminium tetrahydride; chloroformic acid ethyl ester; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
2: Passerini reaction;
DOI:10.1016/j.bmcl.2005.12.013