4-(4-METHYL-1,4-DIAZEPAN-1-YL)BENZALDEHYDE 97

Base Information

• Chemical Name: 4-(4-METHYL-1,4-DIAZEPAN-1-YL)BENZALDEHYDE 97
• CAS No.: 166438-86-4
• Molecular Formula: C₁₃H₁₈N₂O
• Molecular Weight: 218.299
• Hs Code.: 2933990090
• Mol file: 166438-86-4.mol

Synonyms:4-(4-METHYL-1,4-DIAZEPAN-1-YL)BENZALDEHYDE;4-(4-METHYLPERHYDRO-1,4-DIAZEPIN-1-YL)BENZALDEHYDE;4-(4-METHYL-1,4-DIAZEPAN-1-YL)BENZALDEHYDE 97;4-(4-Methyl-1,4-diazepan-1-yl)benzaldehyde 97%

Chemical Property of 4-(4-METHYL-1,4-DIAZEPAN-1-YL)BENZALDEHYDE 97

Chemical Property:

• Vapor Pressure: 1.45E-05mmHg at 25°C
• Melting Point: 44-46
• Boiling Point: 366.6°Cat760mmHg
• Flash Point: 160.1°C
• PSA: 23.55000
• Density: 1.079g/cm³
• LogP: 1.64390

Purity/Quality:

98%min ^*data from raw suppliers

4-(4-Methyl-1,4-diazepan-1-yl)benzaldehyde 97% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C

MSDS Files:

Useful:

Technology Process of 4-(4-METHYL-1,4-DIAZEPAN-1-YL)BENZALDEHYDE 97

There total 3 articles about 4-(4-METHYL-1,4-DIAZEPAN-1-YL)BENZALDEHYDE 97 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

[4-(4-methylperhydro-1,4-diazepin-1-yl)phenyl]methanol (898289-58-2) → 4-(4-methyl-1,4-diazepan-1-yl)benzaldehyde (166438-86-4)

Guidance literature:

With potassium carbonate; In n-heptane; at 80 ℃; for 24h; under 750.075 Torr;

DOI:10.1016/j.chempr.2021.12.001

Reference yield:

4-(4-Methyl-1,4-diazepan-1-yl)benzonitrile (166438-80-8) → 4-(4-methyl-1,4-diazepan-1-yl)benzaldehyde (166438-86-4)

Guidance literature:

aluminum nickel; In formic acid;

Reference yield:

→ 4-(4-methyl-1,4-diazepan-1-yl)benzaldehyde (166438-86-4)

Guidance literature:

With potassium carbonate; In water; at 100 ℃; for 12h;

upstream raw materials:

4-(4-Methyl-1,4-diazepan-1-yl)benzonitrile

[4-(4-methylperhydro-1,4-diazepin-1-yl)phenyl]methanol

Refernces

• 1、 -. "2-PHENYLIMIDAZO[4,5-B]PYRIDIN-7-AMINE DERIVATES USEFUL AS INHIBITORS OF MAMMALIAN TYROSINE KINASE ROR1 ACTIVITY". Page/Page column 86; 87-88. . Retrieved 2018/03/26.