((C₆H₅)3P)2Ni(C₂H)Br

Base Information

Chemical Name:((C₆H₅)3P)2Ni(C₂H)Br
CAS No.:85233-95-0
Molecular Formula:C₃₈H₃₁BrNiP₂
Molecular Weight:688.206
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)3P)2Ni(C<sub>2</sub>H)Br

Synonyms:((C₆H₅)3P)2Ni(C₂H)Br

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((C₆H₅)3P)2Ni(C₂H)Br

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Technology Process of ((C₆H₅)3P)2Ni(C₂H)Br

There total 1 articles about ((C₆H₅)3P)2Ni(C₂H)Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.1%

: 36673-36-6,111408-20-9,14126-37-5,54053-52-0
dibromobis(triphenylphosphine)nickel(II)

: 74-86-2,25067-58-7
acetylene

: 85233-95-0
((C₆H₅)3P)2Ni(C₂H)Br

Guidance literature:: With triethylamine; In tetrahydrofuran; to (Ph3P)2NiBr2 in THF added Et3N at -5°C, C2H2 introduced, reacted for ca. 0.5 h; filtered after ca. 5 h at -20°C, digested with cold MeOH/H2O, dried in high vac.; elem. anal.;
DOI:10.1016/S0022-328X(00)98511-5

Reference yield: 96.0%

: 85233-95-0
((C₆H₅)3P)2Ni(C₂H)Br

: 85233-96-1
((C₆H₅)3P)2Ni(C₂H)Br(CO)

Guidance literature:: With carbon monoxide; In diethyl ether; educt suspended in ether at -30°C, stirred under CO (1 bar) for ca. 3 h; filtered at -78°C, dried in high vac.; elem. anal.;
DOI:10.1016/S0022-328X(00)98511-5