10-dicyclohexylsulfamoyl-D-isobornyl (S)(-)-4-chlorophenylsulfinylacetate

Base Information

Chemical Name:10-dicyclohexylsulfamoyl-D-isobornyl (S)(-)-4-chlorophenylsulfinylacetate
CAS No.:125416-27-5
Molecular Formula:C₃₀H₄₄ClNO₅S₂
Molecular Weight:598.268
Hs Code.:

Synonyms:10-dicyclohexylsulfamoyl-D-isobornyl (S)(-)-4-chlorophenylsulfinylacetate

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Chemical Property of 10-dicyclohexylsulfamoyl-D-isobornyl (S)(-)-4-chlorophenylsulfinylacetate

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Technology Process of 10-dicyclohexylsulfamoyl-D-isobornyl (S)(-)-4-chlorophenylsulfinylacetate

There total 10 articles about 10-dicyclohexylsulfamoyl-D-isobornyl (S)(-)-4-chlorophenylsulfinylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 125382-47-0
10-dicyclohexylsulfamoyl-D-isobornyl 4-chlorophenylsulfenylacetate

: 125416-26-4,125416-27-5
10-dicyclohexylsulfamoyl-D-isobornyl 4-chlorophenylsulfinylacetate

Guidance literature:: With dihydrogen peroxide; acetic acid; at 25 ℃; for 24h;
DOI:10.1016/S0040-4020(01)82313-9

Reference yield:

: 96303-88-7
(-)-10-dicyclohexylsulfamoyl-D-isoborneol

: 125416-27-5
10-dicyclohexylsulfamoyl-D-isobornyl (S)(-)-4-chlorophenylsulfinylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: quinoline / toluene / 52 h / 0 °C

2: 1.) LDA / 1.) THF, hexane, -78 deg C, 30 min; 2.) THF, hexane, a.) -78 deg C, 45 min; b.) -23 deg C, 45 h

With quinoline; lithium diisopropyl amide; In toluene;
DOI:10.1016/S0040-4039(00)99351-1

Reference yield:

: 96303-88-7
(-)-10-dicyclohexylsulfamoyl-D-isoborneol

: 125416-26-4,125416-27-5
10-dicyclohexylsulfamoyl-D-isobornyl 4-chlorophenylsulfinylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / pyridine, 4-DMAP / CH₂Cl₂ / 1) 0 deg C, 1 h, 2) 25 deg C, 24 h

2: 76 percent / 40percent aq tetrabutylammonium hydroxide / benzene / 3 h / 25 °C

3: 92 percent / 30percent aq H₂O₂, glacial acetic acid / 24 h / 25 °C

With pyridine; dmap; tetra(n-butyl)ammonium hydroxide; dihydrogen peroxide; acetic acid; In dichloromethane; benzene;
DOI:10.1016/S0040-4020(01)82313-9