(2Z)-5-[4-(acetyloxy)-3,5-dimethylbenzyl]-3-butyl-2-{[2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzoyl]imino}-2,3-dihydro[1,3]thiazolo[4,5-c]pyridin-5-ium bromide

Base Information

Chemical Name:(2Z)-5-[4-(acetyloxy)-3,5-dimethylbenzyl]-3-butyl-2-{[2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzoyl]imino}-2,3-dihydro[1,3]thiazolo[4,5-c]pyridin-5-ium bromide
CAS No.:1311318-92-9
Molecular Formula:Br*C₃₂H₃₅F₃N₃O₅S
Molecular Weight:710.612
Hs Code.:

(2Z)-5-[4-(acetyloxy)-3,5-dimethylbenzyl]-3-butyl-2-{[2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzoyl]imino}-2,3-dihydro[1,3]thiazolo[4,5-c]pyridin-5-ium bromide

Synonyms:(2Z)-5-[4-(acetyloxy)-3,5-dimethylbenzyl]-3-butyl-2-{[2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzoyl]imino}-2,3-dihydro[1,3]thiazolo[4,5-c]pyridin-5-ium bromide

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Chemical Property of (2Z)-5-[4-(acetyloxy)-3,5-dimethylbenzyl]-3-butyl-2-{[2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzoyl]imino}-2,3-dihydro[1,3]thiazolo[4,5-c]pyridin-5-ium bromide

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Technology Process of (2Z)-5-[4-(acetyloxy)-3,5-dimethylbenzyl]-3-butyl-2-{[2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzoyl]imino}-2,3-dihydro[1,3]thiazolo[4,5-c]pyridin-5-ium bromide

There total 6 articles about (2Z)-5-[4-(acetyloxy)-3,5-dimethylbenzyl]-3-butyl-2-{[2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzoyl]imino}-2,3-dihydro[1,3]thiazolo[4,5-c]pyridin-5-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1231955-18-2
N-[(2Z)-3-butyl[1,3]thiazolo[4,5-c]pyridin-2(3H)-ylidene]-2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzamide

: 711-95-5
acetic acid-(4-bromomethyl-2,6-dimethyl-phenyl ester)

: 1311318-92-9
(2Z)-5-[4-(acetyloxy)-3,5-dimethylbenzyl]-3-butyl-2-{[2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzoyl]imino}-2,3-dihydro[1,3]thiazolo[4,5-c]pyridin-5-ium bromide

Guidance literature:: In acetonitrile; at 20 ℃; for 18h;

Reference yield:

: 915920-75-1
4-(hydroxymethyl)-2,6-dimethylphenyl acetate

: 1311318-92-9
(2Z)-5-[4-(acetyloxy)-3,5-dimethylbenzyl]-3-butyl-2-{[2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzoyl]imino}-2,3-dihydro[1,3]thiazolo[4,5-c]pyridin-5-ium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 6 h / 20 °C

2: acetonitrile / 18 h / 20 °C

With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 1232169-35-5,1311319-13-7
2-fluoro-N-(thiazolo[4,5-c]pyridin-2-yl)-5-(trifluoromethyl)benzamide

: 1311318-92-9
(2Z)-5-[4-(acetyloxy)-3,5-dimethylbenzyl]-3-butyl-2-{[2-{[(2S)-2-hydroxypropyl]oxy}-5-(trifluoromethyl)benzoyl]imino}-2,3-dihydro[1,3]thiazolo[4,5-c]pyridin-5-ium bromide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; tetra-(n-butyl)ammonium iodide; tetraethylammonium iodide / toluene / 12 h / Reflux

2.1: sodium hydride / tetrahydrofuran / 0.33 h / 20 °C

2.2: 4 h / 20 °C

3.1: acetonitrile / 18 h / 20 °C

With tetraethylammonium iodide; tetra(n-butyl)ammonium hydrogensulfate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; In tetrahydrofuran; toluene; acetonitrile;