N-((E)-(1S,4R)-5-Hydroxy-1,4-dimethyl-pent-2-enyl)-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-((E)-(1S,4R)-5-Hydroxy-1,4-dimethyl-pent-2-enyl)-4-methyl-benzenesulfonamide
CAS No.:169686-74-2
Molecular Formula:C₁₄H₂₁NO₃S
Molecular Weight:283.392
Hs Code.:

Synonyms:N-((E)-(1S,4R)-5-Hydroxy-1,4-dimethyl-pent-2-enyl)-4-methyl-benzenesulfonamide

Suppliers and Price of N-((E)-(1S,4R)-5-Hydroxy-1,4-dimethyl-pent-2-enyl)-4-methyl-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((E)-(1S,4R)-5-Hydroxy-1,4-dimethyl-pent-2-enyl)-4-methyl-benzenesulfonamide

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Technology Process of N-((E)-(1S,4R)-5-Hydroxy-1,4-dimethyl-pent-2-enyl)-4-methyl-benzenesulfonamide

There total 5 articles about N-((E)-(1S,4R)-5-Hydroxy-1,4-dimethyl-pent-2-enyl)-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 158195-28-9
(E)-(2R,5S)-2-Methyl-5-(toluene-4-sulfonylamino)-hex-3-enoic acid methyl ester

: 169686-74-2
N-((E)-(1S,4R)-5-Hydroxy-1,4-dimethyl-pent-2-enyl)-4-methyl-benzenesulfonamide

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; for 18h; -78 deg C to room temperature;

Reference yield:

: 43188-65-4
methyl (2S,3S)-3-methyl-1-[(4-methylphenyl)sulfonyl]aziridne-2-carboxylate

: 169686-74-2
N-((E)-(1S,4R)-5-Hydroxy-1,4-dimethyl-pent-2-enyl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) DIBAL, 2.) NH₄Cl / 1.) CH₂Cl₂, toluene, -78 deg C, 0.5 h, 2.) -78 deg C to 0 deg C, 2 h

2: 92 percent / CuCN / tetrahydrofuran; diethyl ether / 1.) 0 deg C, 15 min, 2.) -78 deg C, 30 min

3: 47 percent / DIBAL / CH₂Cl₂; hexane / 18 h / -78 deg C to room temperature

With diisobutylaluminium hydride; ammonium chloride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;

Reference yield:

: 159518-55-5
(3S)-Methyl-N-p-toluolsulfonylaziridin-(2R)-carbonsaeuremethylester

: 169686-74-2
N-((E)-(1S,4R)-5-Hydroxy-1,4-dimethyl-pent-2-enyl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) DIBAL, 2.) NH₄Cl / 1.) CH₂Cl₂, toluene, -78 deg C, 1 h, 2.) -78 deg C to room temperature, 18 h

2: 95 percent / ZnCl₂, CuCN / diethyl ether; tetrahydrofuran / 1.) 0 deg C, 10 min, -78 deg C, 5 min, 2.) -78 deg C, 30 min

3: 47 percent / DIBAL / CH₂Cl₂; hexane / 18 h / -78 deg C to room temperature

With diisobutylaluminium hydride; ammonium chloride; zinc(II) chloride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;