5-benzyl-1,3,4-thiadiazol-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:5-benzyl-1,3,4-thiadiazol-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside
CAS No.:1231980-45-2
Molecular Formula:C₂₃H₂₆N₂O₉S₂
Molecular Weight:538.599
Hs Code.:

Synonyms:5-benzyl-1,3,4-thiadiazol-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

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Chemical Property of 5-benzyl-1,3,4-thiadiazol-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

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Technology Process of 5-benzyl-1,3,4-thiadiazol-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

There total 1 articles about 5-benzyl-1,3,4-thiadiazol-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 29546-25-6
2-mercapto-5-benzyl-1,3,4-thiadiazole

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1231980-45-2
5-benzyl-1,3,4-thiadiazol-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

Guidance literature:: 2-mercapto-5-benzyl-1,3,4-thiadiazole; With sodium hydroxide; In water; at 20 ℃;

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide; With benzyltriethylammonium bromide; In dichloromethane; water; at 20 ℃; for 10h; pH=8 - 10;
DOI:10.1002/cjoc.201090120

Reference yield: 90.0%

: 1231980-45-2
5-benzyl-1,3,4-thiadiazol-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

: 1163695-56-4
5-benzyl-1,3,4-thiadiazol-2-yl 1-thio-β-D-glucopyranoside

Guidance literature:: 5-benzyl-1,3,4-thiadiazol-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside; With sodium methylate; In methanol; at 20 ℃; for 5h;

In methanol; at 20 ℃;
DOI:10.1002/cjoc.201090120