C₁₅H₁₄FNO₄S

Base Information

Chemical Name:C₁₅H₁₄FNO₄S
CAS No.:1415115-18-2
Molecular Formula:C₁₅H₁₄FNO₄S
Molecular Weight:323.345
Hs Code.:

C<sub>15</sub>H<sub>14</sub>FNO<sub>4</sub>S

Synonyms:C₁₅H₁₄FNO₄S

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Chemical Property of C₁₅H₁₄FNO₄S

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Technology Process of C₁₅H₁₄FNO₄S

There total 2 articles about C₁₅H₁₄FNO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1-(2-iodophenoxy)propan-2-one

: 1415115-02-4
2-pyridyl fluoroiodomethyl sulfone

: 1415115-18-2
C₁₅H₁₄FNO₄S

Guidance literature:: 2-pyridyl fluoroiodomethyl sulfone; With diethylzinc; In hexane; N,N-dimethyl-formamide; at -30 - -25 ℃; for 0.0833333h; Inert atmosphere;

With copper(l) iodide; In hexane; N,N-dimethyl-formamide; at -15 ℃; for 0.25h; Inert atmosphere;

1-(2-iodophenoxy)propan-2-one; In hexane; N,N-dimethyl-formamide; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1021/ol3029737

Reference yield:

: 1365765-53-2
2-((fluoromethyl)sulfonyl)pyridine

: 1415115-18-2
C₁₅H₁₄FNO₄S

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate; N-iodo-succinimide / N,N-dimethyl-formamide / 0.5 h / 5 °C / Inert atmosphere

2.1: diethylzinc / N,N-dimethyl-formamide; hexane / 0.08 h / -30 - -25 °C / Inert atmosphere

2.2: 0.25 h / -15 °C / Inert atmosphere

2.3: 8 h / 20 °C / Inert atmosphere

With N-iodo-succinimide; potassium tert-butylate; diethylzinc; In hexane; N,N-dimethyl-formamide;
DOI:10.1021/ol3029737