1,1-dimethylethyl <1-<(4-hydroxyphenyl)methyl>-2-oxo-2-<2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)3-oxo-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>-1H-imidazo-<1,2-a>indol010yl>ethyl>carbonic acid ester

Base Information

Chemical Name:1,1-dimethylethyl <1-<(4-hydroxyphenyl)methyl>-2-oxo-2-<2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)3-oxo-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>-1H-imidazo-<1,2-a>indol010yl>ethyl>carbonic acid ester
CAS No.:103241-32-3
Molecular Formula:C₄₅H₄₆N₆O₈
Molecular Weight:798.896
Hs Code.:

1,1-dimethylethyl <1-<(4-hydroxyphenyl)methyl>-2-oxo-2-<2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)3-oxo-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>-1H-imidazo-<1,2-a>indol010yl>ethyl>carbonic acid ester

Synonyms:1,1-dimethylethyl <1-<(4-hydroxyphenyl)methyl>-2-oxo-2-<2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)3-oxo-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>-1H-imidazo-<1,2-a>indol010yl>ethyl>carbonic acid ester

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Chemical Property of 1,1-dimethylethyl <1-<(4-hydroxyphenyl)methyl>-2-oxo-2-<2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)3-oxo-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>-1H-imidazo-<1,2-a>indol010yl>ethyl>carbonic acid ester

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Technology Process of 1,1-dimethylethyl <1-<(4-hydroxyphenyl)methyl>-2-oxo-2-<2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)3-oxo-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>-1H-imidazo-<1,2-a>indol010yl>ethyl>carbonic acid ester

There total 3 articles about 1,1-dimethylethyl <1-<(4-hydroxyphenyl)methyl>-2-oxo-2-<2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)3-oxo-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>-1H-imidazo-<1,2-a>indol010yl>ethyl>carbonic acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 103241-31-2
C₅₂H₅₂N₆O₈

: 103241-32-3
1,1-dimethylethyl <1-<(4-hydroxyphenyl)methyl>-2-oxo-2-<2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)3-oxo-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>-1H-imidazo-<1,2-a>indol010yl>ethyl>carbonic acid ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 23 ℃; for 4.5h; under 2482.3 Torr;
DOI:10.1021/jm00160a024

Reference yield:

: 37662-17-2
symmetric anhydride of Boc-Tyr(Bzl)-OH

: 103241-32-3
1,1-dimethylethyl <1-<(4-hydroxyphenyl)methyl>-2-oxo-2-<2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)3-oxo-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>-1H-imidazo-<1,2-a>indol010yl>ethyl>carbonic acid ester

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 h / Ambient temperature

2: 98 percent / H₂ / Pd/C / ethanol / 4.5 h / 23 °C / 2482.3 Torr

With dmap; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm00160a024

Reference yield:

: 93413-04-8
Asperlicin

: 103241-32-3
1,1-dimethylethyl <1-<(4-hydroxyphenyl)methyl>-2-oxo-2-<2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)3-oxo-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>-1H-imidazo-<1,2-a>indol010yl>ethyl>carbonic acid ester

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 h / Ambient temperature

2: 98 percent / H₂ / Pd/C / ethanol / 4.5 h / 23 °C / 2482.3 Torr

With dmap; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm00160a024