3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone

Base Information

Chemical Name:3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone
CAS No.:1313481-94-5
Molecular Formula:C₂₉H₃₂N₂O₁₂
Molecular Weight:600.579
Hs Code.:

Synonyms:3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone

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Chemical Property of 3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone

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Technology Process of 3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone

There total 1 articles about 3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1164131-49-0
(E)-4-(3,4-dimethoxyphenyl)-1-((2S,3R,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)but-3-en-2-one

: 108-24-7
acetic anhydride

: 107-91-5
cyanoacetic acid amide

: 1313481-94-5
3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone

Guidance literature:: (E)-4-(3,4-dimethoxyphenyl)-1-((2S,3R,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)but-3-en-2-one; cyanoacetic acid amide; With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Inert atmosphere;

With oxygen; In dimethyl sulfoxide;

acetic anhydride; With pyridine; In dimethyl sulfoxide; at 0 ℃;
DOI:10.1016/j.carres.2011.03.006

Reference yield: 68.0%

: 1313481-94-5
3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone

: 1313482-16-4
2-chloro-3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridine

Guidance literature:: 3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone; With trichlorophosphate; In toluene; at 90 - 100 ℃; for 3h;

With ammonia; In water; toluene; pH=7; Cooling with ice containing K₂CO₃;
DOI:10.1016/j.carres.2011.03.006

Reference yield: 64.0%

: 1313481-94-5
3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone

: 1313482-04-0
3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(β-D-glucopyranosyl)methyl]pyridone

Guidance literature:: 3-cyano-4-(3',4'-dimethoxyphenyl)-6-[(2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranosyl)methyl]pyridone; With sodium methylate; In methanol; at 25 ℃;

With hydrogenchloride; In methanol; water; at 0 ℃;
DOI:10.1016/j.carres.2011.03.006