Diethyl 2-[(2,5-dichloroanilino)methylene]malonate

Base Information

Chemical Name:Diethyl 2-[(2,5-dichloroanilino)methylene]malonate
CAS No.:19056-82-7
Molecular Formula:C₁₄H₁₅Cl₂NO₄
Molecular Weight:332.183
Hs Code.:
NSC Number:137121
DSSTox Substance ID:DTXSID10300462
Mol file:19056-82-7.mol

Synonyms:19056-82-7;diethyl 2-[(2,5-dichloroanilino)methylene]malonate;diethyl 2-[(2,5-dichloroanilino)methylidene]propanedioate;Propanedioic acid, 2-[[(2,5-dichlorophenyl)amino]methylene]-, 1,3-diethyl ester;6J-009;1,3-diethyl 2-{[(2,5-dichlorophenyl)amino]methylidene}propanedioate;NSC137121;CBMicro_044543;DTXSID10300462;diethyl {[(2,5-dichlorophenyl)amino]methylidene}propanedioate;MFCD00173375;STK048856;AKOS003230417;NSC 137121;NSC-137121;BIM-0044703.P001;CS-0333741;Diethyl 2-(((2,5-dichlorophenyl)amino)methylene)malonate;1,3-diethyl2-{[(2,5-dichlorophenyl)amino]methylidene}propanedioate

Suppliers and Price of Diethyl 2-[(2,5-dichloroanilino)methylene]malonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Diethyl 2-[(2,5-dichloroanilino)methylene]malonate

Chemical Property:

Vapor Pressure:6.61E-06mmHg at 25°C
Boiling Point:377.7°Cat760mmHg
Flash Point:182.2°C
Density:1.335g/cm³
XLogP3:4.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:331.0378133
Heavy Atom Count:21
Complexity:380

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=CNC1=C(C=CC(=C1)Cl)Cl)C(=O)OCC

Technology Process of Diethyl 2-[(2,5-dichloroanilino)methylene]malonate

There total 2 articles about Diethyl 2-[(2,5-dichloroanilino)methylene]malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-82-9
2,5 dichloroaniline

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 19056-82-7
NSC137121

Guidance literature:: at 115 - 120 ℃; Yield given; 30-60 min;
DOI:10.1002/(SICI)1097-458X(199611)34:11<972::AID-OMR994>3.0.CO;2-9

Reference yield:

: 19056-82-7
NSC137121

Guidance literature:: DOI:10.1021/jm00273a006

Reference yield:

: 19056-82-7
NSC137121

: 185011-95-4,35975-58-7
5,8-dichloro-4-oxo-1,4-dihydroquinoline-3-carboxylic acid ethyl ester

Guidance literature:: With diphenyl ether-biphenyl eutectic; at 250 ℃; for 1h; Yield given;
DOI:10.1002/(SICI)1097-458X(199611)34:11<972::AID-OMR994>3.0.CO;2-9