1-(2-nitrophenyl)-2-(4-pentynamido)ethyl 6-[bis(4-methoxyphenyl)(phenyl)methoxy]hexanoate

Base Information

Chemical Name:1-(2-nitrophenyl)-2-(4-pentynamido)ethyl 6-[bis(4-methoxyphenyl)(phenyl)methoxy]hexanoate
CAS No.:1402719-26-9
Molecular Formula:C₄₀H₄₂N₂O₈
Molecular Weight:678.782
Hs Code.:

Synonyms:1-(2-nitrophenyl)-2-(4-pentynamido)ethyl 6-[bis(4-methoxyphenyl)(phenyl)methoxy]hexanoate

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Chemical Property of 1-(2-nitrophenyl)-2-(4-pentynamido)ethyl 6-[bis(4-methoxyphenyl)(phenyl)methoxy]hexanoate

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Technology Process of 1-(2-nitrophenyl)-2-(4-pentynamido)ethyl 6-[bis(4-methoxyphenyl)(phenyl)methoxy]hexanoate

There total 6 articles about 1-(2-nitrophenyl)-2-(4-pentynamido)ethyl 6-[bis(4-methoxyphenyl)(phenyl)methoxy]hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: triethylammonium 6-[bis(4-methoxyphenyl)ACHTUNGTRENUNG(phenyl)methoxy]hexanoate

: 1402719-22-5
N-[2-hydroxy-2-(2-nitrophenyl)ethyl]-4-pentynamide

: 1402719-26-9
1-(2-nitrophenyl)-2-(4-pentynamido)ethyl 6-[bis(4-methoxyphenyl)(phenyl)methoxy]hexanoate

Guidance literature:: triethylammonium 6-[bis(4-methoxyphenyl)ACHTUNGTRENUNG(phenyl)methoxy]hexanoate; With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

N-[2-hydroxy-2-(2-nitrophenyl)ethyl]-4-pentynamide; In N,N-dimethyl-formamide; at 70 ℃; for 3h;
DOI:10.1002/chem.201103833

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1402719-26-9
1-(2-nitrophenyl)-2-(4-pentynamido)ethyl 6-[bis(4-methoxyphenyl)(phenyl)methoxy]hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 1 h / 20 °C

2.1: methanol; dichloromethane

3.1: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 1 h / 20 °C

3.2: 3 h / 70 °C

With dmap; triethylamine; dicyclohexyl-carbodiimide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103833

Reference yield:

: 35947-93-4
2-azido-1-(2-nitrophenyl)ethan-1-one

: 1402719-26-9
1-(2-nitrophenyl)-2-(4-pentynamido)ethyl 6-[bis(4-methoxyphenyl)(phenyl)methoxy]hexanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / 1,4-dioxane; methanol / 0 - 20 °C

2.1: triphenylphosphine / 0 - 20 °C

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1 h / 20 °C

3.2: 3 h / 20 °C

4.1: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 1 h / 20 °C

4.2: 3 h / 70 °C

With dmap; sodium tetrahydroborate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; triphenylphosphine; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103833