2-oxo-2-(4-(trifluoromethyl)phenyl)ethyl 3-(2,4-dinitrobenzamido)benzoate

Base Information

Chemical Name:2-oxo-2-(4-(trifluoromethyl)phenyl)ethyl 3-(2,4-dinitrobenzamido)benzoate
CAS No.:1187761-09-6
Molecular Formula:C₂₃H₁₄F₃N₃O₈
Molecular Weight:517.375
Hs Code.:

Synonyms:2-oxo-2-(4-(trifluoromethyl)phenyl)ethyl 3-(2,4-dinitrobenzamido)benzoate

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Chemical Property of 2-oxo-2-(4-(trifluoromethyl)phenyl)ethyl 3-(2,4-dinitrobenzamido)benzoate

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Technology Process of 2-oxo-2-(4-(trifluoromethyl)phenyl)ethyl 3-(2,4-dinitrobenzamido)benzoate

There total 4 articles about 2-oxo-2-(4-(trifluoromethyl)phenyl)ethyl 3-(2,4-dinitrobenzamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 906131-02-0
3-((2,4-dinitro)benzamido)benzoic acid

: 383-53-9
2-bromo-1-[4-(trifluoromethyl)phenyl]ethanone

: 1187761-09-6
2-oxo-2-(4-(trifluoromethyl)phenyl)ethyl 3-(2,4-dinitrobenzamido)benzoate

Guidance literature:: 3-((2,4-dinitro)benzamido)benzoic acid; With caesium carbonate; In ethanol; water; pH=6.5;

2-bromo-1-[4-(trifluoromethyl)phenyl]ethanone; In N,N-dimethyl-formamide; for 12h;

Reference yield:

: 99-05-8,159139-79-4
meta-aminobenzoic acid

: 1187761-09-6
2-oxo-2-(4-(trifluoromethyl)phenyl)ethyl 3-(2,4-dinitrobenzamido)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / 16 h / 0 °C

2.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 3 h

3.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 16 h

4.1: caesium carbonate / ethanol; water / pH 6.5

4.2: 12 h

With thionyl chloride; lithium hydroxide monohydrate; water; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water;

Reference yield:

: 4518-10-9
Methyl 3-aminobenzoate

: 1187761-09-6
2-oxo-2-(4-(trifluoromethyl)phenyl)ethyl 3-(2,4-dinitrobenzamido)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 3 h

2.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 16 h

3.1: caesium carbonate / ethanol; water / pH 6.5

3.2: 12 h

With lithium hydroxide monohydrate; water; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water;