C₆₉H₁₁₆O₉

Base Information

Chemical Name:C₆₉H₁₁₆O₉
CAS No.:1424713-02-9
Molecular Formula:C₆₉H₁₁₆O₉
Molecular Weight:1089.67
Hs Code.:

C<sub>69</sub>H<sub>116</sub>O<sub>9</sub>

Synonyms:C₆₉H₁₁₆O₉

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Chemical Property of C₆₉H₁₁₆O₉

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Technology Process of C₆₉H₁₁₆O₉

There total 19 articles about C₆₉H₁₁₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1424713-00-7
C₄₅H₈₄O₉

: 106-95-6
allyl bromide

: 1424713-02-9
C₆₉H₁₁₆O₉

Guidance literature:: C₄₅H₈₄O₉; allyl bromide; With water; tetra-(n-butyl)ammonium iodide; sodium hydroxide; In toluene; at 45 ℃; for 48h;

With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h; Inert atmosphere;

allyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1055/s-0032-1317929

Reference yield:

: C₂₂H₄₀O₅

: 1424713-02-9
C₆₉H₁₁₆O₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrahydrofuran / 12 h / 65 °C

2.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C / Inert atmosphere

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / -10 °C / Inert atmosphere

4.1: sodium; methanol / 1 h / 0 - 20 °C / Inert atmosphere

5.1: pyridine / 72 h / 110 °C

6.1: potassium carbonate; palladium 10% on activated carbon; hydrogen / ethyl acetate / 48 h / 20 °C / 760.05 Torr

7.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

8.2: 0 - 20 °C / Inert atmosphere

9.1: acetic acid / methanol / 48 h / 20 °C

10.1: water; sodium hydroxide; tetra-(n-butyl)ammonium iodide / toluene / 48 h / 45 °C

10.2: 1 h / 0 °C / Inert atmosphere

10.3: 12 h / 0 - 20 °C / Inert atmosphere

With pyridine; methanol; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; water; hydrogen; sodium; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; potassium carbonate; acetic acid; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; toluene; mineral oil; 3.1: |Mitsunobu Displacement / 8.2: |Williamson Ether Synthesis / 10.3: |Williamson Ether Synthesis;
DOI:10.1055/s-0032-1317929

Reference yield:

: 1424712-86-6
C₅₁H₉₀O₁₀

: 1424713-02-9
C₆₉H₁₁₆O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate; palladium 10% on activated carbon; hydrogen / ethyl acetate / 48 h / 20 °C / 760.05 Torr

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: acetic acid / methanol / 48 h / 20 °C

5.1: water; sodium hydroxide; tetra-(n-butyl)ammonium iodide / toluene / 48 h / 45 °C

5.2: 1 h / 0 °C / Inert atmosphere

5.3: 12 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; palladium 10% on activated carbon; water; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; toluene; mineral oil; 3.2: |Williamson Ether Synthesis / 5.3: |Williamson Ether Synthesis;
DOI:10.1055/s-0032-1317929