methyl 4-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetylamino]butyrate

Base Information

• Chemical Name: methyl 4-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetylamino]butyrate
• CAS No.: 171051-12-0
• Molecular Formula: C₃₀H₃₁N₅O₄
• Molecular Weight: 525.607

Synonyms:methyl 4-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetylamino]butyrate

Chemical Property of methyl 4-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetylamino]butyrate

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Technology Process of methyl 4-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetylamino]butyrate

There total 2 articles about methyl 4-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetylamino]butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

methyl γ-aminobutyrate hydrochloride (13031-60-2) + 3-[2-(2-Carboxymethyl-1-cyclohexenyl)-3-oxo-2,3-dihydropyridazin-6-yl]-2-phenylpyrazolo[1,5-a]-pyridine (171050-45-6) → methyl 4-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetylamino]butyrate (171051-12-0)

Guidance literature:

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; dichloromethane; at 20 ℃;

DOI:10.1016/S0968-0896(99)00258-8

Reference yield:

→ methyl 4-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetylamino]butyrate (171051-12-0)

Guidance literature:

Reference yield: 80.0%

methyl 4-[2-[2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenyl]acetylamino]butyrate (171051-12-0) → 3-[2-(2-(N-(3-carboxypropyl)carbamoyl)methyl-1-cyclohexenyl)-3-oxo-2,3-dihydropyridazin-6-yl]-2-phenylpyrazolo[1,5-a]pyridine

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; water; at 20 ℃;

DOI:10.1016/S0968-0896(99)00258-8

upstream raw materials:

methyl γ-aminobutyrate hydrochloride

3-[2-(2-Carboxymethyl-1-cyclohexenyl)-3-oxo-2,3-dihydropyridazin-6-yl]-2-phenylpyrazolo[1,5-a]-pyridine

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