6-(3,4-dimethoxyphenyl)-1,2,3,5,8,8a-hexahydro-7-(4-methoxyphenyl)indolizine

Base Information

Chemical Name:6-(3,4-dimethoxyphenyl)-1,2,3,5,8,8a-hexahydro-7-(4-methoxyphenyl)indolizine
CAS No.:84416-06-8
Molecular Formula:C₂₃H₂₇NO₃
Molecular Weight:365.472
Hs Code.:

Synonyms:6-(3,4-dimethoxyphenyl)-1,2,3,5,8,8a-hexahydro-7-(4-methoxyphenyl)indolizine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(3,4-dimethoxyphenyl)-1,2,3,5,8,8a-hexahydro-7-(4-methoxyphenyl)indolizine

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Technology Process of 6-(3,4-dimethoxyphenyl)-1,2,3,5,8,8a-hexahydro-7-(4-methoxyphenyl)indolizine

There total 8 articles about 6-(3,4-dimethoxyphenyl)-1,2,3,5,8,8a-hexahydro-7-(4-methoxyphenyl)indolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 6-(3,4-dimethoxyphenyl)-7-(4-methoxyphenyl)-1,2,3,7,8,8a-hexahydroindolizine-5-carbonitrile

: 84416-06-8
6-(3,4-dimethoxyphenyl)-1,2,3,5,8,8a-hexahydro-7-(4-methoxyphenyl)indolizine

Guidance literature:: With sodium tetrahydroborate; isopropyl alcohol; at 100 ℃; for 24h; Sealed tube;
DOI:10.1021/acs.orglett.5b03395

Reference yield:

: 5703-21-9
3,4-dimethoxyphenylacetaldehyde

: 84416-06-8
6-(3,4-dimethoxyphenyl)-1,2,3,5,8,8a-hexahydro-7-(4-methoxyphenyl)indolizine

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 0.5 h

2: 2.) sodium borohydride / 1) methanol, 2 h; 2) methanol, 1 h

With sodium tetrahydroborate; In benzene;

Reference yield:

: 132983-29-0
ethyl 2-(4-methoxybenzoyl)-3-oxobutanoate

: 84416-06-8
6-(3,4-dimethoxyphenyl)-1,2,3,5,8,8a-hexahydro-7-(4-methoxyphenyl)indolizine

Guidance literature:: Multi-step reaction with 5 steps

1: sodium acetate / aq. ethanol / 6 h / Heating

2: aq. KOH / 40 h / Ambient temperature

3: 88 percent / catalase, diamine oxidase / 24 h / 27 °C / pH 7.0

4: benzene / 0.5 h

5: 2.) sodium borohydride / 1) methanol, 2 h; 2) methanol, 1 h

With potassium hydroxide; sodium tetrahydroborate; diamine oxidase; sodium acetate; catalase; In ethanol; benzene;