[(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(OP(o-tolyl)3)]

Base Information

• Chemical Name: [(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(OP(o-tolyl)3)]
• CAS No.: 1366181-68-1
• Molecular Formula: C₄₂H₄₂O₆P₂PdS
• Molecular Weight: 843.225

Synonyms:[(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(OP(o-tolyl)3)]

Chemical Property of [(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(OP(o-tolyl)3)]

Chemical Property:

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Technology Process of [(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(OP(o-tolyl)3)]

There total 1 articles about [(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(OP(o-tolyl)3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[{κ2-(P,O)-(2-anisyl)2PC6H4SO2O}Pd(Me)dmso] (1107629-44-6) + tri-o-tolylphosphine oxide (6163-63-9) → [(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(OP(o-tolyl)3)] (1366181-68-1)

Guidance literature:

In dichloromethane-d2; byproducts: dmso; using Schlenk techniques; at 25°C; monitoring by NMR;

DOI:10.1021/om3000339

Reference yield:

[(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato)PdMe(OP(o-tolyl)3)] (1366181-68-1) → [(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato))PdMe](n) (1233194-46-1) + tri-o-tolylphosphine oxide (6163-63-9)

Guidance literature:

In dichloromethane; using Schlenk techniques; at 25°C; monitoring by IR and NMR;

DOI:10.1021/om3000339

upstream raw materials:

[{κ₂-(P,O)-(2-anisyl)₂PC₆H₄SO₂O}Pd(Me)dmso]

tri-o-tolylphosphine oxide

Downstream raw materials:

[(κ2-P,O-2-(bis(2-methoxyphenyl)phosphino)benzenesulfonato))PdMe](n)

tri-o-tolylphosphine oxide

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