Thiophosphoric acid O-(2-chloro-phenyl) ester S-ethyl ester O'-[(2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(9-phenyl-9H-xanthen-9-yloxymethyl)-tetrahydro-furan-3-yl] ester

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Chemical Name:Thiophosphoric acid O-(2-chloro-phenyl) ester S-ethyl ester O'-[(2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(9-phenyl-9H-xanthen-9-yloxymethyl)-tetrahydro-furan-3-yl] ester
CAS No.:128060-46-8
Molecular Formula:C₃₇H₃₄ClN₂O₈PS
Molecular Weight:733.178
Hs Code.:

Thiophosphoric acid O-(2-chloro-phenyl) ester S-ethyl ester O'-[(2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(9-phenyl-9H-xanthen-9-yloxymethyl)-tetrahydro-furan-3-yl] ester

Synonyms:Thiophosphoric acid O-(2-chloro-phenyl) ester S-ethyl ester O'-[(2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(9-phenyl-9H-xanthen-9-yloxymethyl)-tetrahydro-furan-3-yl] ester

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Chemical Property of Thiophosphoric acid O-(2-chloro-phenyl) ester S-ethyl ester O'-[(2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(9-phenyl-9H-xanthen-9-yloxymethyl)-tetrahydro-furan-3-yl] ester

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Technology Process of Thiophosphoric acid O-(2-chloro-phenyl) ester S-ethyl ester O'-[(2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(9-phenyl-9H-xanthen-9-yloxymethyl)-tetrahydro-furan-3-yl] ester

There total 2 articles about Thiophosphoric acid O-(2-chloro-phenyl) ester S-ethyl ester O'-[(2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(9-phenyl-9H-xanthen-9-yloxymethyl)-tetrahydro-furan-3-yl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 128125-29-1
sodium O-(2-chlorophenyl)-S-ethylphosphorothioate

: 69075-29-2
5'-O-pixylthymidine

: 128060-46-8
Thiophosphoric acid O-(2-chloro-phenyl) ester S-ethyl ester O'-[(2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(9-phenyl-9H-xanthen-9-yloxymethyl)-tetrahydro-furan-3-yl] ester

Guidance literature:: With 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In pyridine; at 20 ℃; for 1h;
DOI:10.1016/S0040-4020(01)89215-2

Reference yield:

: 128125-32-6
sodium O-(2-chlorophenyl)phosphorothioate

: 128060-46-8
Thiophosphoric acid O-(2-chloro-phenyl) ester S-ethyl ester O'-[(2R,3S,5R)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-(9-phenyl-9H-xanthen-9-yloxymethyl)-tetrahydro-furan-3-yl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / dimethylformamide / 12 h / 20 °C

2: 95 percent / 1-mesitylenesulfonyl-3-nitro-1,2,4-triazole / pyridine / 1 h / 20 °C

With 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)89215-2