Technology Process of C2HF3O2*C30H40N6O6S
There total 13 articles about C2HF3O2*C30H40N6O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
dichloromethane;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: thiophene; hydrogen / palladium 10% on activated carbon / methanol; di-isopropyl ether
1.2: 0 °C
2.1: hydrogen / palladium 10% on activated carbon / methanol
3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 96 h / 20 °C
4.1: sodium hydroxide; water / tetrahydrofuran; methanol / 4 h / 20 °C
5.1: dichloromethane / 2 h / 20 °C
With
thiophene; sodium hydroxide; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; di-isopropyl ether;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 20 °C
2: hydrogenchloride / ethanol; isopropyl alcohol / 20 h / Heating / reflux
3: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 96 h / 20 °C
5: sodium hydroxide; water / tetrahydrofuran; methanol / 4 h / 20 °C
6: dichloromethane / 2 h / 20 °C
With
hydrogenchloride; sodium hydroxide; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; isopropyl alcohol;