(1S,4S)-2-[2-(diphenylmethoxy)ethyl]-5-t-Boc-2,5-diazabicyclo[2.2.1]heptane

Base Information

Chemical Name:(1S,4S)-2-[2-(diphenylmethoxy)ethyl]-5-t-Boc-2,5-diazabicyclo[2.2.1]heptane
CAS No.:321365-86-0
Molecular Formula:C₂₅H₃₂N₂O₃
Molecular Weight:408.541
Hs Code.:

Synonyms:(1S,4S)-2-[2-(diphenylmethoxy)ethyl]-5-t-Boc-2,5-diazabicyclo[2.2.1]heptane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,4S)-2-[2-(diphenylmethoxy)ethyl]-5-t-Boc-2,5-diazabicyclo[2.2.1]heptane

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Technology Process of (1S,4S)-2-[2-(diphenylmethoxy)ethyl]-5-t-Boc-2,5-diazabicyclo[2.2.1]heptane

There total 1 articles about (1S,4S)-2-[2-(diphenylmethoxy)ethyl]-5-t-Boc-2,5-diazabicyclo[2.2.1]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 153947-34-3
1-iodo-2-diphenylmethoxy-ethane

: 113451-59-5,174823-32-6
(1S,4S)-2,5-Diaza-bicyclo[2.2.1]heptane-2-carboxylic acid tert-butyl ester

: 321365-86-0
(1S,4S)-2-[2-(diphenylmethoxy)ethyl]-5-t-Boc-2,5-diazabicyclo[2.2.1]heptane

Guidance literature:: With potassium carbonate; In tetrahydrofuran; Heating;
DOI:10.1021/jm000300r

Reference yield:

: 321365-86-0
(1S,4S)-2-[2-(diphenylmethoxy)ethyl]-5-t-Boc-2,5-diazabicyclo[2.2.1]heptane

: (1S,4S)-2-(2-Benzhydryloxy-ethyl)-2,5-diaza-bicyclo[2.2.1]heptane

Guidance literature:: With 88percent aq. HCOOH; at 20 ℃;
DOI:10.1021/jm000300r

Reference yield:

: 321365-86-0
(1S,4S)-2-[2-(diphenylmethoxy)ethyl]-5-t-Boc-2,5-diazabicyclo[2.2.1]heptane

: (1S,4S)-2-[2-(diphenylmethoxy)ethyl]-5-(3-phenylpropyl)-2,5-diazabicyclo[2.2.1]heptane

Guidance literature:: Multi-step reaction with 2 steps

1: 88percent aq. HCOOH / 20 °C

2: K₂CO₃ / tetrahydrofuran / Heating

With potassium carbonate; In tetrahydrofuran;
DOI:10.1021/jm000300r