(2S,3S,4R,5S,6S)-3-(benzyloxy)-6-(6-ethyl-3,5-dimethyl-4-oxo-4H-pyran-2-yl)-5-(methoxymethoxy)-2,4-dimethylheptanal

Base Information

Chemical Name:(2S,3S,4R,5S,6S)-3-(benzyloxy)-6-(6-ethyl-3,5-dimethyl-4-oxo-4H-pyran-2-yl)-5-(methoxymethoxy)-2,4-dimethylheptanal
CAS No.:1228104-07-1
Molecular Formula:C₂₇H₃₈O₆
Molecular Weight:458.595
Hs Code.:

Synonyms:(2S,3S,4R,5S,6S)-3-(benzyloxy)-6-(6-ethyl-3,5-dimethyl-4-oxo-4H-pyran-2-yl)-5-(methoxymethoxy)-2,4-dimethylheptanal

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Chemical Property of (2S,3S,4R,5S,6S)-3-(benzyloxy)-6-(6-ethyl-3,5-dimethyl-4-oxo-4H-pyran-2-yl)-5-(methoxymethoxy)-2,4-dimethylheptanal

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Technology Process of (2S,3S,4R,5S,6S)-3-(benzyloxy)-6-(6-ethyl-3,5-dimethyl-4-oxo-4H-pyran-2-yl)-5-(methoxymethoxy)-2,4-dimethylheptanal

There total 1 articles about (2S,3S,4R,5S,6S)-3-(benzyloxy)-6-(6-ethyl-3,5-dimethyl-4-oxo-4H-pyran-2-yl)-5-(methoxymethoxy)-2,4-dimethylheptanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1228104-39-9
2-((2S,3S,4R,5R,6R)-5-(benzyloxy)-7-hydroxy-3-(methoxymethoxy)-4,6-dimethylheptan-2-yl)-6-ethyl-3,5-dimethyl-4H-pyran-4-one

: 1228104-07-1
(2S,3S,4R,5S,6S)-3-(benzyloxy)-6-(6-ethyl-3,5-dimethyl-4-oxo-4H-pyran-2-yl)-5-(methoxymethoxy)-2,4-dimethylheptanal

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja102356j

Reference yield: 79.0%

: 849343-24-4
(3S)-3-[(R)-(6S)-1,4-dioxa-8-thiaspiro[4.5]dec-6-yl(methoxymethoxy)methyl]tetrahydro-4H-thiopyran-4-one

: 1228104-07-1
(2S,3S,4R,5S,6S)-3-(benzyloxy)-6-(6-ethyl-3,5-dimethyl-4-oxo-4H-pyran-2-yl)-5-(methoxymethoxy)-2,4-dimethylheptanal

: 1228104-14-0
2-((2S,3S,4R,5R,6R,7R)-5-(benzyloxy)-7-hydroxy-3-(methoxymethoxy)-7-((3S,5S)-5-((R)-(methoxymethoxy)((S)-1,4-dioxa-8-thiaspiro[4.5]decan-6-yl)methyl)-4-oxotetrahydro-2H-thiopyran-3-yl)-4,6-dimethylheptan-2-yl)-6-ethyl-3,5-dimethyl-4H-pyran-4-one

: 849343-23-3
(-)-(3S)-3-[(R)-(6S)-1,4-dioxa-8-thiaspiro[4.5]dec-6-yl(triethylsilyloxy)methyl]tetrahydro-4H-thiopyran-4-one

Guidance literature:: (3S)-3-[(R)-(6S)-1,4-dioxa-8-thiaspiro[4.5]dec-6-yl(methoxymethoxy)methyl]tetrahydro-4H-thiopyran-4-one; With titanium tetrachloride; In dichloromethane; at -78 ℃; for 0.0333333h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 1.5h; Inert atmosphere;

(2S,3S,4R,5S,6S)-3-(benzyloxy)-6-(6-ethyl-3,5-dimethyl-4-oxo-4H-pyran-2-yl)-5-(methoxymethoxy)-2,4-dimethylheptanal; In dichloromethane; for 3h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ja102356j