C₄₀H₆₀O₅S

Base Information

Chemical Name:C₄₀H₆₀O₅S
CAS No.:195156-10-6
Molecular Formula:C₄₀H₆₀O₅S
Molecular Weight:652.979
Hs Code.:

C<sub>40</sub>H<sub>60</sub>O<sub>5</sub>S

Synonyms:C₄₀H₆₀O₅S

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Chemical Property of C₄₀H₆₀O₅S

Chemical Property:

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Technology Process of C₄₀H₆₀O₅S

There total 2 articles about C₄₀H₆₀O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 104235-58-7
22β-hydroxy-3β,24-isopropylidenedioxyolean-12-ene

: 98-59-9
p-toluenesulfonyl chloride

: 195156-10-6
C₄₀H₆₀O₅S

Guidance literature:: With pyridine; dmap; at 20 ℃;
DOI:10.1016/j.bmc.2005.04.074

Reference yield:

: 104235-76-9
C₃₃H₅₂O₃

: 195156-10-6
C₄₀H₆₀O₅S

Guidance literature:: Multi-step reaction with 2 steps

1: 6 percent / sodium / 2-methyl-propan-2-ol; toluene / 22 h / Heating

2: 100 percent / pyridine; 4-(dimethylamino)pyridine / 20 °C

With pyridine; dmap; sodium; In toluene; tert-butyl alcohol;
DOI:10.1016/j.bmc.2005.04.074

Reference yield:

: 195156-10-6
C₄₀H₆₀O₅S

: 559-70-6
beta-amyrin

Guidance literature:: Multi-step reaction with 8 steps

1.1: 79 percent / lithium triethylborohydride / dimethylsulfoxide / 1 h / 65 °C

2.1: 93 percent / H₂ / Pd/C / CH₂Cl₂; methanol / 20 °C

3.1: pyridine / 5 h / Heating

4.1: 4-(dimethylamino)pyridine / CH₂Cl₂ / 2 h / 20 °C

5.1: 69 percent / HCl / acetone; methanol / 2 h / 60 °C

6.1: 95 percent / pyridinium chlorochromate / CH₂Cl₂ / 1 h / 20 °C

7.1: 77 percent / NaOH / methanol; tetrahydrofuran / 3 h / 20 °C

8.1: NH₂NH₂*H₂O / bis-(2-hydroxy-ethyl) ether; ethanol / 1 h / Heating; Huang-Minlon reduction

8.2: 77 percent / KOH / 2 h / Heating

With pyridine; hydrogenchloride; dmap; sodium hydroxide; hydrogen; lithium triethylborohydride; hydrazine hydrate; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; dimethyl sulfoxide; acetone; diethylene glycol;
DOI:10.1016/j.bmc.2005.04.074