methyl 3-(1-benzyl-4-dodecanoyl-5-methyl-3-phenylpyrrol-2-yl)propionate

Base Information

Chemical Name:methyl 3-(1-benzyl-4-dodecanoyl-5-methyl-3-phenylpyrrol-2-yl)propionate
CAS No.:1357024-38-4
Molecular Formula:C₃₄H₄₅NO₃
Molecular Weight:515.736
Hs Code.:

Synonyms:methyl 3-(1-benzyl-4-dodecanoyl-5-methyl-3-phenylpyrrol-2-yl)propionate

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Chemical Property of methyl 3-(1-benzyl-4-dodecanoyl-5-methyl-3-phenylpyrrol-2-yl)propionate

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Technology Process of methyl 3-(1-benzyl-4-dodecanoyl-5-methyl-3-phenylpyrrol-2-yl)propionate

There total 6 articles about methyl 3-(1-benzyl-4-dodecanoyl-5-methyl-3-phenylpyrrol-2-yl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1357024-36-2
1-(1-benzyl-2-methyl-4-phenylpyrrol-3-yl)dodecan-1-one

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1357024-38-4
methyl 3-(1-benzyl-4-dodecanoyl-5-methyl-3-phenylpyrrol-2-yl)propionate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 72h;
DOI:10.1016/j.ejmech.2011.12.009

Reference yield:

: 1357024-31-7
ethyl 4-dodecanoyl-5-methyl-3-phenylpyrrole-2-carboxylate

: 1357024-38-4
methyl 3-(1-benzyl-4-dodecanoyl-5-methyl-3-phenylpyrrol-2-yl)propionate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide / ethanol; water / 0.5 h / Reflux

2: 0.33 h / 160 - 170 °C

3: tetrabutylammomium bromide; sodium hydroxide / diethyl ether; dichloromethane; water / 3 h / Reflux

4: boron trifluoride diethyl etherate / dichloromethane / 72 h / 20 °C

With boron trifluoride diethyl etherate; tetrabutylammomium bromide; potassium hydroxide; sodium hydroxide; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2011.12.009

Reference yield:

: 1357024-33-9
4-dodecanoyl-5-methyl-3-phenylpyrrole-2-carboxylic acid

: 1357024-38-4
methyl 3-(1-benzyl-4-dodecanoyl-5-methyl-3-phenylpyrrol-2-yl)propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 0.33 h / 160 - 170 °C

2: tetrabutylammomium bromide; sodium hydroxide / diethyl ether; dichloromethane; water / 3 h / Reflux

3: boron trifluoride diethyl etherate / dichloromethane / 72 h / 20 °C

With boron trifluoride diethyl etherate; tetrabutylammomium bromide; sodium hydroxide; In diethyl ether; dichloromethane; water;
DOI:10.1016/j.ejmech.2011.12.009