C₃₈H₄₉N₅O₁₂

Base Information

Chemical Name:C₃₈H₄₉N₅O₁₂
CAS No.:1313375-38-0
Molecular Formula:C₃₈H₄₉N₅O₁₂
Molecular Weight:767.833
Hs Code.:

C<sub>38</sub>H<sub>49</sub>N<sub>5</sub>O<sub>12</sub>

Synonyms:C₃₈H₄₉N₅O₁₂

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Chemical Property of C₃₈H₄₉N₅O₁₂

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Technology Process of C₃₈H₄₉N₅O₁₂

There total 8 articles about C₃₈H₄₉N₅O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1313375-36-8
C₅₄H₆₅N₅O₂₀

: 1313375-38-0
C₃₈H₄₉N₅O₁₂

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/chem.201003402

Reference yield:

: 1071472-86-0
methyl (E)-4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-but-2-enoate

: 1313375-38-0
C₃₈H₄₉N₅O₁₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 8 h / 85 °C / Inert atmosphere

2.1: sodium methylate / methanol / 24 h / 20 °C

3.1: water; lithium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C / Inert atmosphere

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

4.2: 20 °C

5.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 21 h / 20 - 50 °C / Inert atmosphere

6.1: sodium methylate / methanol / 24 h / 20 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; water; sodium methylate; palladium diacetate; sodium hydrogencarbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; 1.1: Heck coupling / 2.1: Zemplen reaction / 6.1: Zemplen reaction;
DOI:10.1002/chem.201003402

Reference yield:

: 53263-18-6,82659-53-8,98920-44-6,98920-46-8,98920-49-1,103773-87-1,98920-48-0
3-(1'-deoxy-2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)prop-1-ene

: 1313375-38-0
C₃₈H₄₉N₅O₁₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / 45 °C / Inert atmosphere

2.1: tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 8 h / 85 °C / Inert atmosphere

3.1: sodium methylate / methanol / 24 h / 20 °C

4.1: water; lithium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C / Inert atmosphere

5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C

5.2: 20 °C

6.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 21 h / 20 - 50 °C / Inert atmosphere

7.1: sodium methylate / methanol / 24 h / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; water; sodium methylate; palladium diacetate; sodium hydrogencarbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 2.1: Heck coupling / 3.1: Zemplen reaction / 7.1: Zemplen reaction;
DOI:10.1002/chem.201003402