Technology Process of C15H17BrO5
There total 5 articles about C15H17BrO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hypochlorite; sodium hydrogencarbonate; potassium bromide;
In
hexane;
at -10 - 20 ℃;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium cyanide / water / 30 - 45 °C
2: sulfuric acid / 20 °C
3: 1H-imidazole / dichloromethane; ethyl acetate / 25 - 30 °C
4: N-Bromosuccinimide / acetone / 0 - 30 °C
5: sodium hydrogencarbonate; sodium hypochlorite; potassium bromide / hexane / -10 - 20 °C
With
1H-imidazole; sodium cyanide; sodium hypochlorite; N-Bromosuccinimide; sulfuric acid; sodium hydrogencarbonate; potassium bromide;
In
hexane; dichloromethane; water; ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1H-imidazole / dichloromethane; ethyl acetate / 25 - 30 °C
2: N-Bromosuccinimide / acetone / 0 - 30 °C
3: sodium hydrogencarbonate; sodium hypochlorite; potassium bromide / hexane / -10 - 20 °C
With
1H-imidazole; sodium hypochlorite; N-Bromosuccinimide; sodium hydrogencarbonate; potassium bromide;
In
hexane; dichloromethane; ethyl acetate; acetone;