3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline hydrochloride

Base Information

Chemical Name:3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline hydrochloride
CAS No.:128960-31-6
Molecular Formula:C₁₉H₁₃BrClN₅O*ClH
Molecular Weight:479.163
Hs Code.:

Synonyms:3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline hydrochloride

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Chemical Property of 3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline hydrochloride

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Technology Process of 3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline hydrochloride

There total 4 articles about 3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 128960-28-1
2-<2-(p-bromobenzylidene)-1-methylhydrazino>-6-chloroquinoxaline 4-oxide

: 920-37-6
2-Chloroacrylonitrile

: 128960-31-6
3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline hydrochloride

: 128960-32-7
3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline

Guidance literature:: In 1,4-dioxane; for 4h; Heating;

Reference yield: 24.0%

: 128960-28-1
2-<2-(p-bromobenzylidene)-1-methylhydrazino>-6-chloroquinoxaline 4-oxide

: 920-37-6
2-Chloroacrylonitrile

: 128960-31-6
3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline hydrochloride

: 128960-32-7
3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline

Guidance literature:: In 1,4-dioxane; Heating;

Reference yield:

: 126983-41-3
6-chloro-2-[1-methyl-2-(2-thienylmethylene)hydrazino]quinoxaline-4-oxide

: 128960-31-6
3-(p-bromophenyl)-8-chloro-5-cyano-4-hydroxy-1-methyl-2,3-dihydro-1H-1,2-diazepino<3,4-b>quinoxaline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / dimethylformamide / 1 h / Heating

2: 16 percent / dioxane / 4 h / Heating

In 1,4-dioxane; N,N-dimethyl-formamide;