(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 3-methyl-but-2-enyl ester

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Chemical Name:(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 3-methyl-but-2-enyl ester
CAS No.:190207-33-1
Molecular Formula:C₁₉H₂₈N₂O₃
Molecular Weight:332.443
Hs Code.:

Synonyms:(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 3-methyl-but-2-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 3-methyl-but-2-enyl ester

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Technology Process of (S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 3-methyl-but-2-enyl ester

There total 3 articles about (S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 3-methyl-but-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 190207-30-8
(S)-2-((S)-2-Allyloxycarbonylamino-3-methyl-butyrylamino)-3-phenyl-propionic acid 3-methyl-but-2-enyl ester

: 190207-33-1
(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 3-methyl-but-2-enyl ester

Guidance literature:: With diethylamine; palladium diacetate; sodium triphenylphosphinotrisulfonate; In water; acetonitrile; for 0.5h; Ambient temperature;
DOI:10.1016/S0040-4039(97)00535-2

Reference yield:

: 115491-96-8
N-allyloxycarbonyl-(L)-valine

: 190207-33-1
(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 3-methyl-but-2-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / tripropylphosphoric anhydride, (iPr)2NEt / dimethylformamide / 0 deg C -> r.t.

2: 83 percent / HNEt₂ / Pd(OAc)2, sodium triphenylphosphinotrisulfonate / acetonitrile; H₂O / 0.5 h / Ambient temperature

With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; diethylamine; N-ethyl-N,N-diisopropylamine; palladium diacetate; sodium triphenylphosphinotrisulfonate; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(97)00535-2

Reference yield:

: 187154-92-3
phenylalanine prenyl ester

: 190207-33-1
(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 3-methyl-but-2-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / tripropylphosphoric anhydride, (iPr)2NEt / dimethylformamide / 0 deg C -> r.t.

2: 83 percent / HNEt₂ / Pd(OAc)2, sodium triphenylphosphinotrisulfonate / acetonitrile; H₂O / 0.5 h / Ambient temperature

With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; diethylamine; N-ethyl-N,N-diisopropylamine; palladium diacetate; sodium triphenylphosphinotrisulfonate; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(97)00535-2