C₂₉H₂₃O₇NCl₄S

Base Information

Chemical Name:C₂₉H₂₃O₇NCl₄S
CAS No.:874364-55-3
Molecular Formula:C₂₉H₂₃Cl₄NO₇S
Molecular Weight:671.382
Hs Code.:

C<sub>29</sub>H<sub>23</sub>O<sub>7</sub>NCl<sub>4</sub>S

Synonyms:C₂₉H₂₃O₇NCl₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₃O₇NCl₄S

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Technology Process of C₂₉H₂₃O₇NCl₄S

There total 4 articles about C₂₉H₂₃O₇NCl₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 404391-07-7
phenyl 3-O-acetyl-4,6-O-benzylidene-2-deoxy-2-(3,4,5,6-tetrachlorophthalimido)-β-D-thioglucopyranoside

: 874364-55-3
C₂₉H₂₃O₇NCl₄S

Guidance literature:: With triethylsilane; trifluoroacetic acid; In tetrahydrofuran; for 2h;
DOI:10.1002/anie.200602699

Reference yield:

: 286018-83-5
phenyl 2-deoxy-2-tetrachlorophthalimido-1-thio-β-D-glucopyranoside

: 874364-55-3
C₂₉H₂₃O₇NCl₄S

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / TsOH*H₂O / dimethylformamide / 16 h / 20 °C

2: 24 g / triethylamine; DMAP / CH₂Cl₂ / 2.5 h / 20 °C

3: 89 percent / Et₃SiH; TFA / tetrahydrofuran / 2 h

With triethylsilane; dmap; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.200602699

Reference yield:

: 217814-68-1
1-phenylsulfenyl-3,4,6-tri-O-acetyl-1,2-dideoxy-2-N-tetrachlorophthalimido-β-D-glucopyranoside

: 874364-55-3
C₂₉H₂₃O₇NCl₄S

Guidance literature:: Multi-step reaction with 4 steps

1: 62 g / NaOMe; MeOH / 1 h / 0 °C

2: 88 percent / TsOH*H₂O / dimethylformamide / 16 h / 20 °C

3: 24 g / triethylamine; DMAP / CH₂Cl₂ / 2.5 h / 20 °C

4: 89 percent / Et₃SiH; TFA / tetrahydrofuran / 2 h

With methanol; triethylsilane; dmap; sodium methylate; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.200602699