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C25H40O2

Base Information
  • Chemical Name:C25H40O2
  • CAS No.:1428957-11-2
  • Molecular Formula:C25H40O2
  • Molecular Weight:372.591
  • Hs Code.:
C<sub>25</sub>H<sub>40</sub>O<sub>2</sub>

Synonyms:C25H40O2

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Chemical Property of C25H40O2
Chemical Property:
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Technology Process of C25H40O2

There total 16 articles about C25H40O2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
diethoxyphosphoryl-acetic acid ethyl ester; With 15-crown-5; sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃;
C21H34O; In tetrahydrofuran; mineral oil; at -40 - 20 ℃;
Guidance literature:
Multi-step reaction with 16 steps
1.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C
1.2: -40 - 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
3.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere
4.1: sodium ethanolate / ethanol / 0 °C
4.2: 16 h / 0 - 20 °C
5.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C
6.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C
6.2: -40 - 20 °C
7.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
8.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere
9.1: sodium ethanolate / ethanol / 0 °C / Inert atmosphere
9.2: 16 h / 0 - 20 °C
10.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C
11.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0.25 h / 0 °C
11.2: -40 - 20 °C
12.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
13.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere
14.1: sodium ethanolate / ethanol / 0 °C
14.2: 16 h / 0 - 20 °C
15.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C
16.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C
16.2: -40 - 20 °C
With lithium aluminium tetrahydride; 15-crown-5; sodium ethanolate; phosphorus tribromide; sodium hydride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; mineral oil;
Guidance literature:
Multi-step reaction with 15 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
2.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere
3.1: sodium ethanolate / ethanol / 0 °C
3.2: 16 h / 0 - 20 °C
4.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C
5.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C
5.2: -40 - 20 °C
6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
7.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere
8.1: sodium ethanolate / ethanol / 0 °C / Inert atmosphere
8.2: 16 h / 0 - 20 °C
9.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C
10.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0.25 h / 0 °C
10.2: -40 - 20 °C
11.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
12.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere
13.1: sodium ethanolate / ethanol / 0 °C
13.2: 16 h / 0 - 20 °C
14.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C
15.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C
15.2: -40 - 20 °C
With lithium aluminium tetrahydride; 15-crown-5; sodium ethanolate; phosphorus tribromide; sodium hydride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; mineral oil;
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