(-)-<(R)-6-heptyl>-p-toluolsulfonat

Base Information

Chemical Name:(-)-<(R)-6-heptyl>-p-toluolsulfonat
CAS No.:133447-61-7
Molecular Formula:C₂₂H₄₀O₄SSi
Molecular Weight:428.709
Hs Code.:

(-)-<(R)-6-<Dimethyl(1,1,2-trimethylpropyl)silyloxy>heptyl>-p-toluolsulfonat

Synonyms:(-)-<(R)-6-heptyl>-p-toluolsulfonat

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Chemical Property of (-)-<(R)-6-heptyl>-p-toluolsulfonat

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Technology Process of (-)-<(R)-6-heptyl>-p-toluolsulfonat

There total 3 articles about (-)-<(R)-6-heptyl>-p-toluolsulfonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 133447-60-6
(-)-(R)-6--1-heptanol

: 98-59-9
p-toluenesulfonyl chloride

: 133447-61-7
(-)-<(R)-6-heptyl>-p-toluolsulfonat

Guidance literature:: With pyridine; at 4 ℃; for 2h;

Reference yield:

: 133447-58-2
(-)-(R)-7-Benzyloxy-2-heptanol

: 133447-61-7
(-)-<(R)-6-heptyl>-p-toluolsulfonat

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / imidazol / dimethylformamide / 16 h

2: 92 percent / H₂, AcOH / 10percent Pd/C / methanol / 0.67 h

3: 88 percent / pyridine / 2 h / 4 °C

With pyridine; 1H-imidazole; hydrogen; acetic acid; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 133447-59-3
(-)-(R)-1-Benzyloxy-6-heptan

: 133447-61-7
(-)-<(R)-6-heptyl>-p-toluolsulfonat

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / H₂, AcOH / 10percent Pd/C / methanol / 0.67 h

2: 88 percent / pyridine / 2 h / 4 °C

With pyridine; hydrogen; acetic acid; palladium on activated charcoal; In methanol;