Technology Process of C18H30O4
There total 9 articles about C18H30O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / dimethyl sulfoxide / 0.25 h / 0 °C
2: methanol; copper diacetate; ammonium chloride / dimethyl sulfoxide / 24 h / 20 °C
3: sodium tetrahydroborate; nickel (II) chloride hexahydrate / methanol / 3 h / 0 - 20 °C
4: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C
5: diisobutylaluminium hydride / dichloromethane / 0.25 h / 0 °C
With
methanol; sodium tetrahydroborate; nickel (II) chloride hexahydrate; copper diacetate; diisobutylaluminium hydride; ammonium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium chloride;
In
methanol; dichloromethane; dimethyl sulfoxide;
1: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.tetlet.2011.03.089
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate; nickel (II) chloride hexahydrate / methanol / 3 h / 0 - 20 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C
3: diisobutylaluminium hydride / dichloromethane / 0.25 h / 0 °C
With
sodium tetrahydroborate; nickel (II) chloride hexahydrate; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine;
In
methanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.03.089
