2-(((tert-butyldimethylsilyl)oxy)methyl)-5-oxo-5,6-dihydro-2H-pyran-2-yl 3,4,5-trifluorobenzoate

Base Information

Chemical Name:2-(((tert-butyldimethylsilyl)oxy)methyl)-5-oxo-5,6-dihydro-2H-pyran-2-yl 3,4,5-trifluorobenzoate
CAS No.:1638115-82-8
Molecular Formula:C₁₉H₂₃F₃O₅Si
Molecular Weight:416.469
Hs Code.:

Synonyms:2-(((tert-butyldimethylsilyl)oxy)methyl)-5-oxo-5,6-dihydro-2H-pyran-2-yl 3,4,5-trifluorobenzoate

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Chemical Property of 2-(((tert-butyldimethylsilyl)oxy)methyl)-5-oxo-5,6-dihydro-2H-pyran-2-yl 3,4,5-trifluorobenzoate

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Technology Process of 2-(((tert-butyldimethylsilyl)oxy)methyl)-5-oxo-5,6-dihydro-2H-pyran-2-yl 3,4,5-trifluorobenzoate

There total 2 articles about 2-(((tert-butyldimethylsilyl)oxy)methyl)-5-oxo-5,6-dihydro-2H-pyran-2-yl 3,4,5-trifluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1377151-82-0
6-(((tert-butyldimethylsilyl)oxy)methyl)-6-hydroxy-2H-pyran-3(6H)-one

: 121602-93-5,255875-61-7
3,4,5-trifluorobenzoic acid

: 1638115-82-8
2-(((tert-butyldimethylsilyl)oxy)methyl)-5-oxo-5,6-dihydro-2H-pyran-2-yl 3,4,5-trifluorobenzoate

Guidance literature:: With dmap; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/anie.201402834

Reference yield:

: 753004-76-1
[5-(tert-butyl-dimethyl-silanyloxymethyl)-furan-2-yl]-methanol

: 1638115-82-8
2-(((tert-butyldimethylsilyl)oxy)methyl)-5-oxo-5,6-dihydro-2H-pyran-2-yl 3,4,5-trifluorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: dmap / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With dmap; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1002/anie.201402834