(3R,4R,5R)-5-(((4-methoxyphenyl)diphenylmethoxy)methyl)tetrahydrofuran-2,3,4-triyl triacetate

Base Information

• Chemical Name: (3R,4R,5R)-5-(((4-methoxyphenyl)diphenylmethoxy)methyl)tetrahydrofuran-2,3,4-triyl triacetate
• CAS No.: 126713-03-9
• Molecular Formula: C₃₁H₃₂O₉
• Molecular Weight: 548.59

Synonyms:(3R,4R,5R)-5-(((4-methoxyphenyl)diphenylmethoxy)methyl)tetrahydrofuran-2,3,4-triyl triacetate

Chemical Property of (3R,4R,5R)-5-(((4-methoxyphenyl)diphenylmethoxy)methyl)tetrahydrofuran-2,3,4-triyl triacetate

Chemical Property:

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Technology Process of (3R,4R,5R)-5-(((4-methoxyphenyl)diphenylmethoxy)methyl)tetrahydrofuran-2,3,4-triyl triacetate

There total 4 articles about (3R,4R,5R)-5-(((4-methoxyphenyl)diphenylmethoxy)methyl)tetrahydrofuran-2,3,4-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

acetic anhydride (108-24-7) + (3R,45,5R)-5-(((4-methoxyphenyl)diphenylmethoxy)methyl)tetrahydrofuran-2,3,4-triol → (3R,4R,5R)-5-(((4-methoxyphenyl)diphenylmethoxy)methyl)tetrahydrofuran-2,3,4-triyl triacetate (126713-03-9)

Guidance literature:

With pyridine; at 20 ℃; for 16h;

Reference yield:

D-Ribose (532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7) + acetic anhydride (108-24-7) + mono-4-methoxytrityl chloride (14470-28-1) → (3R,4R,5R)-5-(((4-methoxyphenyl)diphenylmethoxy)methyl)tetrahydrofuran-2,3,4-triyl triacetate (126713-03-9)

Guidance literature:

With pyridine; Yield given. Multistep reaction; 1) 20 deg C, 24 h, 2) DCM, 20 deg C, 16 h;

DOI:10.1016/0008-6215(90)80033-Y

Reference yield:

mono-4-methoxytrityl chloride (14470-28-1) → (3R,4R,5R)-5-(((4-methoxyphenyl)diphenylmethoxy)methyl)tetrahydrofuran-2,3,4-triyl triacetate (126713-03-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 16 h / 20 °C

2: pyridine / 16 h / 20 °C

With pyridine;

upstream raw materials:

D-Ribose

acetic anhydride

mono-4-methoxytrityl chloride

D-Ribose

Downstream raw materials:

2',3'-diacetyl-N⁴-benzoylcytidine

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