3-BUTYL-1,1,2-TRIMETHYL-1H-BENZ[E]INDOLIUM IODIDE

Base Information

• Chemical Name: 3-BUTYL-1,1,2-TRIMETHYL-1H-BENZ[E]INDOLIUM IODIDE
• CAS No.: 137107-72-3
• Molecular Formula: C19H24 N . I
• Molecular Weight: 393.311
• Mol file: 137107-72-3.mol

Synonyms:1H-Benz[e]indolium,3-butyl-1,1,2-trimethyl-, iodide (9CI)

Chemical Property of 3-BUTYL-1,1,2-TRIMETHYL-1H-BENZ[E]INDOLIUM IODIDE

Chemical Property:

• PSA: 3.01000
• LogP: 1.99880

Purity/Quality:

98%Min ^*data from raw suppliers

3-Butyl-1,1,2-trimethyl-1H-benz[e]indoliumiodide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BUTYL-1,1,2-TRIMETHYL-1H-BENZ[E]INDOLIUM IODIDE

There total 5 articles about 3-BUTYL-1,1,2-TRIMETHYL-1H-BENZ[E]INDOLIUM IODIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-iodo-butane (542-69-8) + 2,3,3-trimethylbenzo[e]indole (41532-84-7) → 3-butyl-1,1,2-trimethyl-1H-benzo[e]indol-3-ium iodide (137107-72-3)

Guidance literature:

In nitromethane; Inert atmosphere; Reflux;

Reference yield: 62.0%

→ 3-butyl-1,1,2-trimethyl-1H-benzo[e]indol-3-ium iodide (137107-72-3)

Guidance literature:

In butanone; at 70 ℃; for 18h;

Reference yield:

3-methyl-butan-2-one (563-80-4) → 3-butyl-1,1,2-trimethyl-1H-benzo[e]indol-3-ium iodide (137107-72-3)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / 24 h / 100 °C

2: acetonitrile / 100 °C

With acetic acid; In acetonitrile; 1: |Fischer Indole Synthesis;

DOI:10.3390/molecules23020226

upstream raw materials:

1-iodo-butane

2,3,3-trimethylbenzo[e]indole

2-naphthylhydrazine hydrochloride

3-methyl-butan-2-one

Downstream raw materials:

C₂₇H₃₁ClNO⁽¹⁺⁾*I^(1-)

3-butyl-2-((1E,3E)-3-(3-butyl-1,1-dimethyl-1H-benzo[e]indol-2(3H)-ylidene)prop-1-en-1-yl)-1,1-dimethyl-1H-benzo[e]indol-3-ium iodide

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