N-(3-methylbut-2-en-1-yl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

Base Information

Chemical Name:N-(3-methylbut-2-en-1-yl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide
CAS No.:1381869-93-7
Molecular Formula:C₁₄H₁₆N₂O₄S
Molecular Weight:308.358
Hs Code.:

Synonyms:N-(3-methylbut-2-en-1-yl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

Suppliers and Price of N-(3-methylbut-2-en-1-yl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-methylbut-2-en-1-yl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

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Technology Process of N-(3-methylbut-2-en-1-yl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

There total 3 articles about N-(3-methylbut-2-en-1-yl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1578267-79-4
C₁₁H₁₄N₂O₄S

: 106-96-7
propargyl bromide

: 1381869-93-7
N-(3-methylbut-2-en-1-yl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1021/jo500045n

Reference yield:

: 503-60-6
3,3-dimethyl-allyl chloride

: 1381869-93-7
N-(3-methylbut-2-en-1-yl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 12 h / 60 °C / Schlenk technique; Inert atmosphere

2: potassium carbonate / acetonitrile / 12 h / 80 °C / Inert atmosphere; Schlenk technique

With potassium carbonate; In acetone; acetonitrile;
DOI:10.1021/jo500045n

Reference yield:

: 5455-59-4
2-Nitrobenzenesulfonamide

: 1381869-93-7
N-(3-methylbut-2-en-1-yl)-2-nitro-N-(prop-2-yn-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 12 h / 60 °C / Schlenk technique; Inert atmosphere

2: potassium carbonate / acetonitrile / 12 h / 80 °C / Inert atmosphere; Schlenk technique

With potassium carbonate; In acetone; acetonitrile;
DOI:10.1021/jo500045n